D-myo-Inositol, 2,4,6-tris-O-(phenylmethyl)-, 3,5-bisbis(phenylmethyl) phosphate

Base Information

Chemical Name:D-myo-Inositol, 2,4,6-tris-O-(phenylmethyl)-, 3,5-bisbis(phenylmethyl) phosphate
CAS No.:227177-04-0
Molecular Formula:C55H56 O12 P2
Molecular Weight:970.97
Hs Code.:

Synonyms:D-myo-Inositol, 2,4,6-tris-O-(phenylmethyl)-, 3,5-bisbis(phenylmethyl) phosphate

Suppliers and Price of D-myo-Inositol, 2,4,6-tris-O-(phenylmethyl)-, 3,5-bisbis(phenylmethyl) phosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-myo-Inositol, 2,4,6-tris-O-(phenylmethyl)-, 3,5-bisbis(phenylmethyl) phosphate

Chemical Property:

PSA：157.06000
LogP:11.97090

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of D-myo-Inositol, 2,4,6-tris-O-(phenylmethyl)-, 3,5-bisbis(phenylmethyl) phosphate

There total 11 articles about D-myo-Inositol, 2,4,6-tris-O-(phenylmethyl)-, 3,5-bisbis(phenylmethyl) phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 226889-61-8
1D-2,4,6-tri-O-benzyl-1-O-(4'-methoxybenzyl)-myo-inositol 3,5-bis(dibenzyl phosphate)

: 227177-04-0
1D-2,4,6-tri-O-benzyl-myo-inositol 3,5-bis(dibenzyl phosphate)

Guidance literature:: With ammonium cerium(IV) nitrate; water; In acetonitrile; at 0 ℃; for 0.75h;

Reference yield: 91.0%

: (R)-5-Oxo-tetrahydro-furan-2-carboxylic acid (1R,2S,3S,4R,5R,6S)-2,4,6-tris-benzyloxy-3,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

: 227177-04-0
1D-2,4,6-tri-O-benzyl-myo-inositol 3,5-bis(dibenzyl phosphate)

Guidance literature:: With ammonia; In methanol; Ambient temperature;
DOI:10.1016/S0040-4039(98)01422-1

Reference yield:

: 100-39-0
benzyl bromide

: 227177-04-0
1D-2,4,6-tri-O-benzyl-myo-inositol 3,5-bis(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 9 steps

1: NaH / dimethylformamide / 0 - 20 °C

2: CH₂Cl₂; hexane / 0 - 20 °C

3: 89 percent / NaH, tetrabutylammonium iodide / dimethylformamide / 1.) r.t., 2 h, 2.) r.t., 20 h

4: 92 percent / HCl, H₂O / CHCl₃; methanol / 10 h / 25 °C

5: 24 percent / pyridine, DMAP / CH₂Cl₂ / 24 h / 0 °C

6: 90 percent / LiOH, H₂O / tetrahydrofuran / 19 h / Ambient temperature

7: 1H-tetrazole / CH₂Cl₂ / 1.33 h / Ambient temperature

8: mCPBA / CH₂Cl₂ / 1.) -78 deg C, 1 h, 2.) r.t., 1 h

9: 93 percent / (NH₄)2Ce(NO₂)6, H₂O / acetonitrile / 0.75 h / 0 °C

With pyridine; 1H-tetrazole; hydrogenchloride; dmap; lithium hydroxide; ammonium cerium(IV) nitrate; water; tetra-(n-butyl)ammonium iodide; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; chloroform; N,N-dimethyl-formamide; acetonitrile;