myo-Inositol, 1,5-O-ethylidene-3-O-(4-methoxyphenyl)methyl-2,4,6-tris-O-(phenylmethyl)-, stereoisomer

Base Information

Chemical Name:myo-Inositol, 1,5-O-ethylidene-3-O-(4-methoxyphenyl)methyl-2,4,6-tris-O-(phenylmethyl)-, stereoisomer
CAS No.:227177-02-8
Molecular Formula:C₃₇H₄₀O₇
Molecular Weight:596.72
Hs Code.:

Synonyms:myo-Inositol, 1,5-O-ethylidene-3-O-(4-methoxyphenyl)methyl-2,4,6-tris-O-(phenylmethyl)-, stereoisomer

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Chemical Property of myo-Inositol, 1,5-O-ethylidene-3-O-(4-methoxyphenyl)methyl-2,4,6-tris-O-(phenylmethyl)-, stereoisomer

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Technology Process of myo-Inositol, 1,5-O-ethylidene-3-O-(4-methoxyphenyl)methyl-2,4,6-tris-O-(phenylmethyl)-, stereoisomer

There total 8 articles about myo-Inositol, 1,5-O-ethylidene-3-O-(4-methoxyphenyl)methyl-2,4,6-tris-O-(phenylmethyl)-, stereoisomer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 824-94-2
p-methoxybenzyl chloride

: 227177-05-1
(1R,5S,6S,7R,8S,9R)-6,8,9-Tris-benzyloxy-3-methyl-2,4-dioxa-bicyclo[3.3.1]nonan-7-ol

: 227177-02-8
(1S,5R,6S,7R,8S,9R)-6,8,9-Tris-benzyloxy-7-(4-methoxy-benzyloxy)-3-methyl-2,4-dioxa-bicyclo[3.3.1]nonane

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; 0 deg C, 1 h to RT, 14 h;
DOI:10.1016/S0040-4039(98)00941-1

Reference yield: 97.0%

: 824-94-2
p-methoxybenzyl chloride

: 227177-05-1
(±)-2,4,6-tri-O-benzyl-1,5-O-ethyldiene myo-inositol

: 227177-02-8
(1R*,3R*,5S*,6R*,7R*,8R*,9R*)-6,8,9-tris(benzyloxy)-7-<(4'-methoxyphenyl)methoxy>-3-methyl-2,4-dioxabicyclo<3.3.1>nonane

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/b913399b

Reference yield:

: 100-39-0
benzyl bromide

: 227177-02-8
(1S,5R,6S,7R,8S,9R)-6,8,9-Tris-benzyloxy-7-(4-methoxy-benzyloxy)-3-methyl-2,4-dioxa-bicyclo[3.3.1]nonane

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / NaH / dimethylformamide / 0 deg C, 2 h to RT, 18 h

2: 87 percent / CH₂Cl₂ / 0 deg C, 3 h to RT, 4 h

3: 98 percent / NaH / dimethylformamide / 0 deg C, 1 h to RT, 14 h

With sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(98)00941-1