tert-butyl [(1S)-1-benzyl-2-({2-[(hydroxyamino)carbonyl]-1-benzothien-6-yl}amino)ethyl]carbamate

Base Information

Chemical Name:tert-butyl [(1S)-1-benzyl-2-({2-[(hydroxyamino)carbonyl]-1-benzothien-6-yl}amino)ethyl]carbamate
CAS No.:913653-79-9
Molecular Formula:C₂₃H₂₇N₃O₄S
Molecular Weight:441.551
Hs Code.:

Synonyms:tert-butyl [(1S)-1-benzyl-2-({2-[(hydroxyamino)carbonyl]-1-benzothien-6-yl}amino)ethyl]carbamate

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Chemical Property of tert-butyl [(1S)-1-benzyl-2-({2-[(hydroxyamino)carbonyl]-1-benzothien-6-yl}amino)ethyl]carbamate

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Technology Process of tert-butyl [(1S)-1-benzyl-2-({2-[(hydroxyamino)carbonyl]-1-benzothien-6-yl}amino)ethyl]carbamate

There total 4 articles about tert-butyl [(1S)-1-benzyl-2-({2-[(hydroxyamino)carbonyl]-1-benzothien-6-yl}amino)ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: C₂₄H₂₈N₂O₄S

: 913653-79-9
tert-butyl [(1S)-1-benzyl-2-({2-[(hydroxyamino)carbonyl]-1-benzothien-6-yl}amino)ethyl]carbamate

Guidance literature:: With hydroxylamine; In water; N,N-dimethyl-formamide; for 48h;

Reference yield:

: 34084-88-3
methyl 6-nitrobenzo[b]thiophene--2--carboxylate

: 913653-79-9
tert-butyl [(1S)-1-benzyl-2-({2-[(hydroxyamino)carbonyl]-1-benzothien-6-yl}amino)ethyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / N,N-dimethyl-formamide / 96 h / 20 °C

2: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane

3: hydroxylamine / water; N,N-dimethyl-formamide / 48 h

With hydrogen; hydroxylamine; sodium tris(acetoxy)borohydride; acetic acid; palladium 10% on activated carbon; In water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 528-75-6
2,4-dinitrobenzaldehyde

: 913653-79-9
tert-butyl [(1S)-1-benzyl-2-({2-[(hydroxyamino)carbonyl]-1-benzothien-6-yl}amino)ethyl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 - 50 °C

2: hydrogen / palladium 10% on activated carbon / N,N-dimethyl-formamide / 96 h / 20 °C

3: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane

4: hydroxylamine / water; N,N-dimethyl-formamide / 48 h

With hydrogen; hydroxylamine; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; palladium 10% on activated carbon; In water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;