Methyl 6-nitro-1-benzothiophene-2-carboxylate, 2-(Methoxycarbonyl)-6-nitro-1-benzothiophene

Base Information

• Chemical Name: Methyl 6-nitro-1-benzothiophene-2-carboxylate, 2-(Methoxycarbonyl)-6-nitro-1-benzothiophene
• CAS No.: 34084-88-3
• Molecular Formula: C₁₀H₇NO₄S
• Molecular Weight: 237.236
• Hs Code.: 2934999090
• Mol file: 34084-88-3.mol

Synonyms:6-Nitrobenzothiophen-2-carbonsaeure-methylester;6-Nitrobenzthiophen-2-carbonsaeuremethylester;6-nitrobenzothiophene-2-carboxylic acid methyl ester;

Chemical Property of Methyl 6-nitro-1-benzothiophene-2-carboxylate, 2-(Methoxycarbonyl)-6-nitro-1-benzothiophene

Chemical Property:

• Vapor Pressure: 2.16E-06mmHg at 25°C
• Boiling Point: 393.2oC at 760 mmHg
• Flash Point: 191.6oC
• PSA: 100.36000
• Density: 1.457g/cm3
• LogP: 3.11930
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Methyl 6-nitrobenzo[b]thiophene-2-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 6-nitro-1-benzothiophene-2-carboxylate, 2-(Methoxycarbonyl)-6-nitro-1-benzothiophene

There total 4 articles about Methyl 6-nitro-1-benzothiophene-2-carboxylate, 2-(Methoxycarbonyl)-6-nitro-1-benzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

methanol (67-56-1) + 6-nitrobenzo[b]thiophene-2-carboxylic acid (19983-42-7) → methyl 6-nitrobenzo[b]thiophene--2--carboxylate (34084-88-3)

Guidance literature:

With thionyl chloride; In methanol; at 0 - 60 ℃;

Reference yield: 78.0%

2,4-dinitrobenzaldehyde (528-75-6) + Methyl thioglycolate (2365-48-2) → methyl 6-nitrobenzo[b]thiophene--2--carboxylate (34084-88-3)

Guidance literature:

With triethylamine; In dimethyl sulfoxide; at 20 - 110 ℃; for 14h;

Reference yield: 70.0%

Methyl thioglycolate (2365-48-2) + 4-nitro-2-fluorobenzaldehyde (157701-72-9) → methyl 6-nitrobenzo[b]thiophene--2--carboxylate (34084-88-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 15h;

DOI:10.1016/j.ejmech.2019.04.024

upstream raw materials:

2,4-dinitrobenzaldehyde

Methyl thioglycolate

methanol

6-nitrobenzo[b]thiophene-2-carboxylic acid

Downstream raw materials:

6-dibenzylamino-benzo[b]thiophene-2-carboxylic acid methyl ester

6-dibenzylamino-benzo[b]thiophene-2-carboxylic acid hydroxyamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 34084-88-3 Methyl 6-nitro-1-benzothiophene-2-carboxylate, 2-(Methoxycarbonyl)-6-nitro-1-benzothiophene

Send

Send

Metric Ton KG G Pound L ML

Send

Send