2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dichloro-phenyl]-5,5-dimethyl-[1,3,2] dioxaborinane

Base Information

Chemical Name:2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dichloro-phenyl]-5,5-dimethyl-[1,3,2] dioxaborinane
CAS No.:959766-36-0
Molecular Formula:C₁₇H₂₇BCl₂O₃Si
Molecular Weight:389.202
Hs Code.:

Synonyms:2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dichloro-phenyl]-5,5-dimethyl-[1,3,2] dioxaborinane

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Chemical Property of 2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dichloro-phenyl]-5,5-dimethyl-[1,3,2] dioxaborinane

Chemical Property:

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Technology Process of 2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dichloro-phenyl]-5,5-dimethyl-[1,3,2] dioxaborinane

There total 2 articles about 2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dichloro-phenyl]-5,5-dimethyl-[1,3,2] dioxaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 959766-35-9
tert-butyl-(2,4-dichloro-5-iodophenoxy)-dimethyl-silane

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 959766-36-0
2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dichloro-phenyl]-5,5-dimethyl-[1,3,2] dioxaborinane

Guidance literature:: tert-butyl-(2,4-dichloro-5-iodophenoxy)-dimethyl-silane; With n-butyllithium; Triisopropyl borate; In tetrahydrofuran; hexane; toluene; at -78 ℃; Inert atmosphere;

2,2-Dimethyl-1,3-propanediol; In tetrahydrofuran; hexane; toluene; at 0 - 25 ℃;

Reference yield:

: 5419-55-6
Triisopropyl borate

: 959766-35-9
tert-butyl-(2,4-dichloro-5-iodophenoxy)-dimethyl-silane

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 959766-36-0
2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dichloro-phenyl]-5,5-dimethyl-[1,3,2] dioxaborinane

Guidance literature:: Triisopropyl borate; tert-butyl-(2,4-dichloro-5-iodophenoxy)-dimethyl-silane; With n-butyllithium; In tetrahydrofuran; hexane; toluene; at -78 ℃; for 0.583333h;

2,2-Dimethyl-1,3-propanediol; In tetrahydrofuran; hexane; toluene; at 0 - 20 ℃; for 8h;

Reference yield:

: 959766-36-0
2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dichloro-phenyl]-5,5-dimethyl-[1,3,2] dioxaborinane

: 959766-37-1
4-benzylsulfanyl-6-chloro-[1,3,5]triazin-2-ylamine

: 959766-38-2
5-(4-amino-6-benzylsulfanyl-[1,3,5] triazin-2-yl)-2,4-dichloro-phenol

Guidance literature:: With sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 80 ℃; for 4h;