Undec-10-eneselenoic acid Se-phenyl ester

Base Information

• Chemical Name: Undec-10-eneselenoic acid Se-phenyl ester
• CAS No.: 73335-20-3
• Molecular Formula: C₁₇H₂₄OSe
• Molecular Weight: 323.337
• Mol file: 73335-20-3.mol

Synonyms:Undec-10-eneselenoic acid Se-phenyl ester

Chemical Property of Undec-10-eneselenoic acid Se-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Undec-10-eneselenoic acid Se-phenyl ester

There total 2 articles about Undec-10-eneselenoic acid Se-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

10-undecenoic acid hydrazide (5458-77-5) + benzeneseleninic acid (6996-92-5) → Undec-10-eneselenoic acid Se-phenyl ester (73335-20-3)

Guidance literature:

With triphenylphosphine; In dichloromethane; for 0.5h;

DOI:10.1021/jo00321a008

Reference yield:

→ Undec-10-eneselenoic acid Se-phenyl ester (73335-20-3)

Guidance literature:

CH2=CH-(CH2)8-CO-NH-NH2, C6H5SeO2H (2);

DOI:10.1016/S0040-4039(01)86379-6

Reference yield: 55.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + Undec-10-eneselenoic acid Se-phenyl ester (73335-20-3) → 1-dodecen-11-one (5009-33-6) + bis(phenylseleno)methane (20343-90-2) + 1-phenylseleno-11-dodecen-2-one (83756-36-9)

Guidance literature:

copper(l) iodide; In diethyl ether;

DOI:10.1016/S0040-4020(01)96714-6

upstream raw materials:

10-undecenoic acid hydrazide

benzeneseleninic acid

Downstream raw materials:

1-dodecen-11-one

bis(phenylseleno)methane

1-phenylseleno-11-dodecen-2-one

diphenyl diselenide