N₁,N₃-bis(1,1-dimethylethyl)-5-(phenylmethoxy)-1,3-benzenedicarboxamide

Base Information

• Chemical Name: N₁,N₃-bis(1,1-dimethylethyl)-5-(phenylmethoxy)-1,3-benzenedicarboxamide
• CAS No.: 1185753-87-0
• Molecular Formula: C₂₃H₃₀N₂O₃
• Molecular Weight: 382.503
• Mol file: 1185753-87-0.mol

Synonyms:N₁,N₃-bis(1,1-dimethylethyl)-5-(phenylmethoxy)-1,3-benzenedicarboxamide

Chemical Property of N₁,N₃-bis(1,1-dimethylethyl)-5-(phenylmethoxy)-1,3-benzenedicarboxamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N₁,N₃-bis(1,1-dimethylethyl)-5-(phenylmethoxy)-1,3-benzenedicarboxamide

There total 1 articles about N₁,N₃-bis(1,1-dimethylethyl)-5-(phenylmethoxy)-1,3-benzenedicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

5-(benzyloxy)benzene-1,3-dicarboxylic acid (114274-39-4) + tert-butylamine (75-64-9) → N1,N3-bis(1,1-dimethylethyl)-5-(phenylmethoxy)-1,3-benzenedicarboxamide (1185753-87-0)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1039/b900843h

Reference yield: 99.0%

N1,N3-bis(1,1-dimethylethyl)-5-(phenylmethoxy)-1,3-benzenedicarboxamide (1185753-87-0) → N,N'-di-tert-butyl-5-hydroxy-isophthalamide (866959-41-3)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 50 ℃; under 760.051 Torr;

DOI:10.1016/j.tetlet.2012.06.063

upstream raw materials:

5-(benzyloxy)benzene-1,3-dicarboxylic acid

tert-butylamine

Downstream raw materials:

N,N'-di-tert-butyl-5-hydroxy-isophthalamide