8,26-dibenzyl-3,6,10,13,21,24,28,31,37,38-decaaza-tricyclo[31.3.1.1^15,19]octatriaconta-1⁽³⁷⁾,15,17,19⁽³⁸⁾,33,35-hexaene-7,9,25,27-tetraone

Base Information

• Chemical Name: 8,26-dibenzyl-3,6,10,13,21,24,28,31,37,38-decaaza-tricyclo[31.3.1.1^15,19]octatriaconta-1⁽³⁷⁾,15,17,19⁽³⁸⁾,33,35-hexaene-7,9,25,27-tetraone
• CAS No.: 793710-50-6
• Molecular Formula: C₄₂H₅₄N₁₀O₄
• Molecular Weight: 762.955

Synonyms:8,26-dibenzyl-3,6,10,13,21,24,28,31,37,38-decaaza-tricyclo[31.3.1.1^15,19]octatriaconta-1⁽³⁷⁾,15,17,19⁽³⁸⁾,33,35-hexaene-7,9,25,27-tetraone

Chemical Property of 8,26-dibenzyl-3,6,10,13,21,24,28,31,37,38-decaaza-tricyclo[31.3.1.1^15,19]octatriaconta-1⁽³⁷⁾,15,17,19⁽³⁸⁾,33,35-hexaene-7,9,25,27-tetraone

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Technology Process of 8,26-dibenzyl-3,6,10,13,21,24,28,31,37,38-decaaza-tricyclo[31.3.1.1^15,19]octatriaconta-1⁽³⁷⁾,15,17,19⁽³⁸⁾,33,35-hexaene-7,9,25,27-tetraone

There total 1 articles about 8,26-dibenzyl-3,6,10,13,21,24,28,31,37,38-decaaza-tricyclo[31.3.1.1^15,19]octatriaconta-1⁽³⁷⁾,15,17,19⁽³⁸⁾,33,35-hexaene-7,9,25,27-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2,6-Pyridinedicarboxaldehyde (5431-44-7) + 6-benzyl-1,4,8,11-tetraazaundecane-5,7-dione (160618-33-7) → 8,26-dibenzyl-3,6,10,13,21,24,28,31,37,38-decaaza-tricyclo[31.3.1.115,19]octatriaconta-1(37),15,17,19(38),33,35-hexaene-7,9,25,27-tetraone (793710-50-6)

Guidance literature:

2,6-Pyridinedicarboxaldehyde; 6-benzyl-1,4,8,11-tetraazaundecane-5,7-dione; In acetonitrile; at 20 ℃;

With sodium tetrahydroborate; In acetonitrile;

DOI:10.1002/anie.200460568

Reference yield:

copper(II) bis(trifluoromethanesulfonate) (34946-82-2) + 8,26-dibenzyl-3,6,10,13,21,24,28,31,37,38-decaaza-tricyclo[31.3.1.115,19]octatriaconta-1(37),15,17,19(38),33,35-hexaene-7,9,25,27-tetraone (793710-50-6) → [Cu2((C6H5)CH2CHC(O)NCH2CH2NHCH2(C5H3N)CH2NHCH2CH2NC(O))2] (799271-63-9)

Guidance literature:

With potassium hydroxide; In ethanol; water; soln. of Cu(CF3SO3)2 and macrocycle in water/ethanol at pH 11.5 slowly evapd.; elem. anal.;

DOI:10.1002/anie.200460568

Reference yield:

water (7732-18-5) + copper(II) bis(trifluoromethanesulfonate) (34946-82-2) + 8,26-dibenzyl-3,6,10,13,21,24,28,31,37,38-decaaza-tricyclo[31.3.1.115,19]octatriaconta-1(37),15,17,19(38),33,35-hexaene-7,9,25,27-tetraone (793710-50-6) → 2Cu(2+)*((C6H5)CH2CHC(O)NHCH2CH2NHCH2C5H3NCH2NHCH2CH2NHC(O))2*OH(1-)*3CF3SO3(1-)*5H2O=[Cu2(C42H54N10O4)OH](CF3SO3)3*5H2O

Guidance literature:

With potassium hydroxide; In ethanol; water; soln. of Cu(CF3SO3)2 and macrocycle in water/ethanol at pH 7.0 slowly evapd.; elem. anal.;

DOI:10.1002/anie.200460568

upstream raw materials:

2,6-Pyridinedicarboxaldehyde

6-benzyl-1,4,8,11-tetraazaundecane-5,7-dione

Downstream raw materials:

[Cu₂(((C₆H₅)CH₂CHC(O)NHCH₂CH₂NHCH₂C₅H₃NCH₂NHCH₂CH₂NHC(O))2)(C₃H₃N₂)]⁽³⁺⁾

[Cu₂((C₆H₅)CH₂CHC(O)NCH₂CH₂NHCH₂(C₅H₃N)CH₂NHCH₂CH₂NC(O))2]

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