(±)-N'-(2-((2,4-dimethoxybenzyl)amino)-8-methoxyquinazolin-4-yl)-3-hydroxybutanehydrazide

Base Information

Chemical Name:(±)-N'-(2-((2,4-dimethoxybenzyl)amino)-8-methoxyquinazolin-4-yl)-3-hydroxybutanehydrazide
CAS No.:1616709-33-1
Molecular Formula:C₂₂H₂₇N₅O₅
Molecular Weight:441.487
Hs Code.:

Synonyms:(±)-N'-(2-((2,4-dimethoxybenzyl)amino)-8-methoxyquinazolin-4-yl)-3-hydroxybutanehydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (±)-N'-(2-((2,4-dimethoxybenzyl)amino)-8-methoxyquinazolin-4-yl)-3-hydroxybutanehydrazide

Chemical Property:

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Technology Process of (±)-N'-(2-((2,4-dimethoxybenzyl)amino)-8-methoxyquinazolin-4-yl)-3-hydroxybutanehydrazide

There total 2 articles about (±)-N'-(2-((2,4-dimethoxybenzyl)amino)-8-methoxyquinazolin-4-yl)-3-hydroxybutanehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20781-20-8
2,4-Dimethoxybenzylamine

: 1616709-32-0
(±)-N'-(2-chloro-8-methoxyquinazolin-4-yl)-3-hydroxybutanehydrazide

: 1616709-33-1
(±)-N'-(2-((2,4-dimethoxybenzyl)amino)-8-methoxyquinazolin-4-yl)-3-hydroxybutanehydrazide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; at 100 ℃; for 16h;

Reference yield:

: 3177-80-8
2-amino-3-methoxybenzoic acid

: 1616709-33-1
(±)-N'-(2-((2,4-dimethoxybenzyl)amino)-8-methoxyquinazolin-4-yl)-3-hydroxybutanehydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / water / 5 h / 55 - 60 °C

1.2: 20 °C

2.1: trichlorophosphate / 16 h / 105 °C

3.1: N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 16 h / 60 °C

4.1: N-ethyl-N,N-diisopropylamine / 16 h / 100 °C

With acetic acid; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In 1,4-dioxane; water;