6-Isoquinolinol,7-methoxy-(9CI)

Base Information

• Chemical Name: 6-Isoquinolinol,7-methoxy-(9CI)
• CAS No.: 226958-59-4
• Molecular Formula: C₁₀H₉NO₂
• Molecular Weight: 175.187
• Mol file: 226958-59-4.mol

Synonyms:NSC 235792

Chemical Property of 6-Isoquinolinol,7-methoxy-(9CI)

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

7-methoxy-6-Isoquinolinol 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-Isoquinolinol,7-methoxy-(9CI)

There total 2 articles about 6-Isoquinolinol,7-methoxy-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-{[(Z)-2,2-Dimethoxy-ethylimino]-methyl}-2-methoxy-phenol → 7-methoxyisoquinolin-6-ol (226958-59-4)

Guidance literature:

With boron trifluoride diethyl etherate; trifluoroacetic anhydride; In toluene; for 72h; Ambient temperature;

DOI:10.1080/00397919908086144

Reference yield:

vanillin (121-33-5,8014-42-4) → 7-methoxyisoquinolin-6-ol (226958-59-4)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 5 h / Heating

2: 21 g / BF₃*Et₂O, (CF₃CO)2O / toluene / 72 h / Ambient temperature

With boron trifluoride diethyl etherate; trifluoroacetic anhydride; In toluene;

DOI:10.1080/00397919908086144

upstream raw materials:

vanillin

Refernces