Technology Process of C9H11NO4
There total 4 articles about C9H11NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanol; sodium hydroxide;
In
water;
at 0 ℃;
for 0.333333h;
DOI:10.1002/ejoc.201001629
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine; dmap / dichloromethane / 0.5 h / 20 °C
2: methanol; sodium hydroxide / water / 0.33 h / 0 °C
With
pyridine; methanol; dmap; sodium hydroxide;
In
dichloromethane; water;
DOI:10.1002/ejoc.201001629
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / Reflux
1.2: 0.5 h / 20 °C
1.3: pH 6
2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 4 h / 20 °C
3.1: pyridine; dmap / dichloromethane / 0.5 h / 20 °C
4.1: methanol; sodium hydroxide / water / 0.33 h / 0 °C
With
pyridine; methanol; dmap; palladium 10% on activated carbon; hydrogen; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide;
In
dichloromethane; water; ethyl acetate;
DOI:10.1002/ejoc.201001629