tert-butyl (mesityl)dichlorogermane

Base Information

Chemical Name:tert-butyl (mesityl)dichlorogermane
CAS No.:115879-26-0
Molecular Formula:C₁₃H₂₀Cl₂Ge
Molecular Weight:319.798
Hs Code.:

Synonyms:tert-butyl (mesityl)dichlorogermane

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Chemical Property of tert-butyl (mesityl)dichlorogermane

Chemical Property:

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Technology Process of tert-butyl (mesityl)dichlorogermane

There total 3 articles about tert-butyl (mesityl)dichlorogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2,2'-azobis(2-methylpropionitrile)

: 126529-90-6
tert-butyl (mesityl)dihydrogermane

: 115879-26-0
tert-butyl (mesityl)dichlorogermane

Guidance literature:: In tetrachloromethane; A mixt. of tert-butyl (mesityl) germane, CCl4 and azo bis(isobutyronitrile) was heated at 80°C for 3 h in an autoclave.; elimination of CCl4 and CHCl3 in vacuo, recrystn. in pentane, elem. anal.;

Reference yield: 31.0%

: 1184-92-5
tert-butyltrichlorogermane

: 2633-66-1
2-mesitylmagnesium bromide

: 115879-26-0
tert-butyl (mesityl)dichlorogermane

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; benzene; addn. of MesMgBr/THF to a soln. of BuGeCl3/benzene at room temp., reflux for 12h, allowing to cool, hydrolyzed with dilute HCl; extraction with ether, Kugelrohr distn. (100°C, 0.02 Torr); elem. anal.;

Reference yield:

: 114806-82-5
(2,4,6-trimethylphenyl)trichlorogermane

: 115879-26-0
tert-butyl (mesityl)dichlorogermane

Guidance literature:: Multi-step reaction with 2 steps

1: t-butyl lithium; hydrochloric acid; LiAlH₄ / diethyl ether; pentane

2: tetrachloromethane

With t-butyl lithium; hydrochloric acid; LiAlH₄; In tetrachloromethane; diethyl ether; pentane;