benzyl (3S,5R)-3-(tert-butoxycarbonylamino)-5-methoxy-piperidine-1-carboxylate

Base Information

Chemical Name:benzyl (3S,5R)-3-(tert-butoxycarbonylamino)-5-methoxy-piperidine-1-carboxylate
CAS No.:1187055-50-0
Molecular Formula:C₁₉H₂₈N₂O₅
Molecular Weight:364.442
Hs Code.:

Synonyms:benzyl (3S,5R)-3-(tert-butoxycarbonylamino)-5-methoxy-piperidine-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (3S,5R)-3-(tert-butoxycarbonylamino)-5-methoxy-piperidine-1-carboxylate

Chemical Property:

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Technology Process of benzyl (3S,5R)-3-(tert-butoxycarbonylamino)-5-methoxy-piperidine-1-carboxylate

There total 10 articles about benzyl (3S,5R)-3-(tert-butoxycarbonylamino)-5-methoxy-piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1187055-49-7
(3S,5R)-benzyl 3-azido-5-methoxypiperidine-1-carboxylate

: 1187055-50-0
benzyl (3S,5R)-3-(tert-butoxycarbonylamino)-5-methoxy-piperidine-1-carboxylate

Guidance literature:: (3S,5R)-benzyl 3-azido-5-methoxypiperidine-1-carboxylate; With ammonium hydroxide; trimethylphosphane; In pyridine; at 20 ℃; for 4h;

di-tert-butyl dicarbonate; With sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; water; at 0 - 20 ℃;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: benzyl (3S,5R)-3-amino-5-methoxy-piperidine-1-carboxylate

: 1187055-50-0
benzyl (3S,5R)-3-(tert-butoxycarbonylamino)-5-methoxy-piperidine-1-carboxylate

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; water; at 0 - 20 ℃; for 2h;

Reference yield:

: 1187055-36-2,1785642-46-7
benzyl (3S,5R)-3-(tert-butoxycarbonylamino)-5-hydroxypiperidine-1-carboxylate

: 74-88-4
methyl iodide

: 1187055-50-0
benzyl (3S,5R)-3-(tert-butoxycarbonylamino)-5-methoxy-piperidine-1-carboxylate

Guidance literature:: benzyl (3S,5R)-3-(tert-butoxycarbonylamino)-5-hydroxypiperidine-1-carboxylate; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; mineral oil; at 15 ℃; for 1h;