Carbonic acid (2R,3S,4R,5R,6S)-6-allyloxy-5-allyloxycarbonylamino-4-(4-azido-3-chloro-benzyloxy)-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester 3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyl ester

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Chemical Name:Carbonic acid (2R,3S,4R,5R,6S)-6-allyloxy-5-allyloxycarbonylamino-4-(4-azido-3-chloro-benzyloxy)-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester 3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyl ester
CAS No.:873848-26-1
Molecular Formula:C₄₆H₆₇ClN₄O₁₉
Molecular Weight:1015.51
Hs Code.:

Carbonic acid (2R,3S,4R,5R,6S)-6-allyloxy-5-allyloxycarbonylamino-4-(4-azido-3-chloro-benzyloxy)-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester 3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyl ester

Synonyms:Carbonic acid (2R,3S,4R,5R,6S)-6-allyloxy-5-allyloxycarbonylamino-4-(4-azido-3-chloro-benzyloxy)-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester 3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyl ester

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Chemical Property of Carbonic acid (2R,3S,4R,5R,6S)-6-allyloxy-5-allyloxycarbonylamino-4-(4-azido-3-chloro-benzyloxy)-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester 3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyl ester

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Technology Process of Carbonic acid (2R,3S,4R,5R,6S)-6-allyloxy-5-allyloxycarbonylamino-4-(4-azido-3-chloro-benzyloxy)-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester 3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyl ester

There total 8 articles about Carbonic acid (2R,3S,4R,5R,6S)-6-allyloxy-5-allyloxycarbonylamino-4-(4-azido-3-chloro-benzyloxy)-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester 3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: [(2S,3R,4R,5S,6R)-2-Allyloxy-4-(4-azido-3-chloro-benzyloxy)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl]-carbamic acid allyl ester

: 873848-25-0
carbonic acid 3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyl ester 4-nitro-phenyl ester

: 873848-26-1
Carbonic acid (2R,3S,4R,5R,6S)-6-allyloxy-5-allyloxycarbonylamino-4-(4-azido-3-chloro-benzyloxy)-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester 3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyl ester

Guidance literature:: With dmap; In dichloromethane;
DOI:10.1055/s-2005-872269

Reference yield:

: 873848-07-8
3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzoic acid

: 873848-26-1
Carbonic acid (2R,3S,4R,5R,6S)-6-allyloxy-5-allyloxycarbonylamino-4-(4-azido-3-chloro-benzyloxy)-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester 3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / LiAlH₄

2: 58 percent / DMAP / CH₂Cl₂

With dmap; lithium aluminium tetrahydride; In dichloromethane;
DOI:10.1055/s-2005-872269

Reference yield:

: 112-35-6,95507-80-5
triethylene glucol monomethyl ether

: 873848-26-1
Carbonic acid (2R,3S,4R,5R,6S)-6-allyloxy-5-allyloxycarbonylamino-4-(4-azido-3-chloro-benzyloxy)-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester 3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 100 percent / Et₃N / CH₂Cl₂

2: 78 percent / NaH / dimethylformamide

3: 100 percent / Et₃N / CH₂Cl₂

4: NaI; K₂CO₃ / 50 °C

5: aq. NaOH / dimethylformamide

6: 95 percent / LiAlH₄

7: 58 percent / DMAP / CH₂Cl₂

With dmap; sodium hydroxide; lithium aluminium tetrahydride; sodium hydride; potassium carbonate; triethylamine; sodium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2005-872269