(S)-(Z)-[2-(5-triethylsilyloxy-2-methylene-cyclohexylidene)ethyl]diphenylphosphineoxide

Base Information

Chemical Name:(S)-(Z)-[2-(5-triethylsilyloxy-2-methylene-cyclohexylidene)ethyl]diphenylphosphineoxide
CAS No.:1202355-78-9
Molecular Formula:C₂₇H₃₇O₂PSi
Molecular Weight:452.649
Hs Code.:

Synonyms:(S)-(Z)-[2-(5-triethylsilyloxy-2-methylene-cyclohexylidene)ethyl]diphenylphosphineoxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(Z)-[2-(5-triethylsilyloxy-2-methylene-cyclohexylidene)ethyl]diphenylphosphineoxide

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Technology Process of (S)-(Z)-[2-(5-triethylsilyloxy-2-methylene-cyclohexylidene)ethyl]diphenylphosphineoxide

There total 1 articles about (S)-(Z)-[2-(5-triethylsilyloxy-2-methylene-cyclohexylidene)ethyl]diphenylphosphineoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 994-30-9
triethylsilyl chloride

: 1236132-10-7
(S)-(Z)-[2-(5-hydroxy-2-methylene-cyclohexylidene)ethyl]di-phenylphosphineoxide

: 1202355-78-9
(S)-(Z)-[2-(5-triethylsilyloxy-2-methylene-cyclohexylidene)ethyl]diphenylphosphineoxide

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.04.051

Reference yield: 84.0%

: 1202355-78-9
(S)-(Z)-[2-(5-triethylsilyloxy-2-methylene-cyclohexylidene)ethyl]diphenylphosphineoxide

: 1236132-15-2
11α-(7-ethoxycarbonylhept-1-yl)-25-triethylsilyloxy-de-A,B-cholest-8-one

: 1236132-16-3
3β-O-triethylsilyl-11α-(7-ethoxycarbonylhept-1-yl)-25-triethylsilyloxy-vitamin D3

Guidance literature:: (S)-(Z)-[2-(5-triethylsilyloxy-2-methylene-cyclohexylidene)ethyl]diphenylphosphineoxide; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.666667h; Inert atmosphere;

11α-(7-ethoxycarbonylhept-1-yl)-25-triethylsilyloxy-de-A,B-cholest-8-one; In tetrahydrofuran; at -78 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.04.051

Reference yield:

: 1202355-78-9
(S)-(Z)-[2-(5-triethylsilyloxy-2-methylene-cyclohexylidene)ethyl]diphenylphosphineoxide

: 1202355-92-7
C₁₉H₂₃⁽²⁾H₉O

: C₃₄H₄₉⁽²⁾H₉OSi

Guidance literature:: (S)-(Z)-[2-(5-triethylsilyloxy-2-methylene-cyclohexylidene)ethyl]diphenylphosphineoxide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

C₁₉H₂₃⁽²⁾H₉O; In tetrahydrofuran; hexane; at -78 ℃; for 2.5h;