Trifluoro-acetic acid 4-[(1R,2S)-1-ethyl-2-(4-fluorosulfonyl-phenyl)-butyl]-phenyl ester

Base Information

Chemical Name:Trifluoro-acetic acid 4-[(1R,2S)-1-ethyl-2-(4-fluorosulfonyl-phenyl)-butyl]-phenyl ester
CAS No.:76412-42-5
Molecular Formula:C₂₀H₂₀F₄O₄S
Molecular Weight:432.436
Hs Code.:

Synonyms:Trifluoro-acetic acid 4-[(1R,2S)-1-ethyl-2-(4-fluorosulfonyl-phenyl)-butyl]-phenyl ester

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Chemical Property of Trifluoro-acetic acid 4-[(1R,2S)-1-ethyl-2-(4-fluorosulfonyl-phenyl)-butyl]-phenyl ester

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Technology Process of Trifluoro-acetic acid 4-[(1R,2S)-1-ethyl-2-(4-fluorosulfonyl-phenyl)-butyl]-phenyl ester

There total 3 articles about Trifluoro-acetic acid 4-[(1R,2S)-1-ethyl-2-(4-fluorosulfonyl-phenyl)-butyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84-16-2,26614-21-1
hexestrol

: 76412-42-5
Trifluoro-acetic acid 4-[(1R,2S)-1-ethyl-2-(4-fluorosulfonyl-phenyl)-butyl]-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) K₂CO₃, 2.) H₂ / 2.) 5percent Pd/C / 1.) acetone, reflux, 17 h, 2.) ethanol, 37 psi, 35 deg C

2: 98 percent / triethylamine / benzene / 1.08 h / 0 - 20 °C

3: fluorosulfonic acid / 0.5 h / -23 - 0 °C

With hydrogen; fluorosulphonic acid; potassium carbonate; triethylamine; palladium on activated charcoal; In benzene;
DOI:10.1021/jm00136a013

Reference yield:

: 3929-22-4,5776-73-8,5776-74-9
deoxyhexestrol

: 76412-42-5
Trifluoro-acetic acid 4-[(1R,2S)-1-ethyl-2-(4-fluorosulfonyl-phenyl)-butyl]-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / triethylamine / benzene / 1.08 h / 0 - 20 °C

2: fluorosulfonic acid / 0.5 h / -23 - 0 °C

With fluorosulphonic acid; triethylamine; In benzene;
DOI:10.1021/jm00136a013

Reference yield:

: deoxyhexestrol trifluoroacetate

: 76412-05-0
p-(fluorosulfonyl)deoxyhexestrol

: 76412-42-5
Trifluoro-acetic acid 4-[(1R,2S)-1-ethyl-2-(4-fluorosulfonyl-phenyl)-butyl]-phenyl ester

Guidance literature:: With fluorosulphonic acid; at -23 - 0 ℃; for 0.5h; Title compound not separated from byproducts;
DOI:10.1021/jm00136a013