1-(4-methoxybenzyl)-4-(benzylamino)-N-(2,2-dimethoxyethyl)-1H-imidazole-5-carboxamide

Base Information

Chemical Name:1-(4-methoxybenzyl)-4-(benzylamino)-N-(2,2-dimethoxyethyl)-1H-imidazole-5-carboxamide
CAS No.:1450627-98-1
Molecular Formula:C₂₃H₂₈N₄O₄
Molecular Weight:424.5
Hs Code.:

Synonyms:1-(4-methoxybenzyl)-4-(benzylamino)-N-(2,2-dimethoxyethyl)-1H-imidazole-5-carboxamide

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Chemical Property of 1-(4-methoxybenzyl)-4-(benzylamino)-N-(2,2-dimethoxyethyl)-1H-imidazole-5-carboxamide

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Technology Process of 1-(4-methoxybenzyl)-4-(benzylamino)-N-(2,2-dimethoxyethyl)-1H-imidazole-5-carboxamide

There total 4 articles about 1-(4-methoxybenzyl)-4-(benzylamino)-N-(2,2-dimethoxyethyl)-1H-imidazole-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₆N₄O₄

: 1450627-98-1
1-(4-methoxybenzyl)-4-(benzylamino)-N-(2,2-dimethoxyethyl)-1H-imidazole-5-carboxamide

Guidance literature:: With sodium cyanoborohydride; In methanol; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1016/j.bmc.2013.06.069

Reference yield:

: 1450627-92-5
1-(4-methoxybenzyl)-4-nitro-1H-imidazole-5-carboxylic acid

: 1450627-98-1
1-(4-methoxybenzyl)-4-(benzylamino)-N-(2,2-dimethoxyethyl)-1H-imidazole-5-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / Reflux; Inert atmosphere

1.2: 2 h / 20 °C

2.1: palladium on activated charcoal; hydrogen / methanol / 5 h / 2068.65 Torr

3.1: trifluoroacetic acid / methanol / 20 °C / Inert atmosphere

4.1: sodium cyanoborohydride / methanol / 8 h / 20 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; sodium cyanoborohydride; 1,1'-carbonyldiimidazole; trifluoroacetic acid; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmc.2013.06.069

Reference yield:

: 1450627-93-6
1-(4-methoxybenzyl)-N-(2,2-dimethoxyethyl)-4-nitro-1H-imidazole-5-carboxamide

: 1450627-98-1
1-(4-methoxybenzyl)-4-(benzylamino)-N-(2,2-dimethoxyethyl)-1H-imidazole-5-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: palladium on activated charcoal; hydrogen / methanol / 5 h / 2068.65 Torr

2: trifluoroacetic acid / methanol / 20 °C / Inert atmosphere

3: sodium cyanoborohydride / methanol / 8 h / 20 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; sodium cyanoborohydride; trifluoroacetic acid; In methanol;
DOI:10.1016/j.bmc.2013.06.069