(S)-5-Methyl-2-oxo-2-(3-phenyl-propyl)-2λ⁵-[1,3,2]dioxaphospholan-4-one

Base Information

Chemical Name:(S)-5-Methyl-2-oxo-2-(3-phenyl-propyl)-2λ⁵-[1,3,2]dioxaphospholan-4-one
CAS No.:1025941-45-0
Molecular Formula:C₁₂H₁₅O₄P
Molecular Weight:254.222
Hs Code.:

(S)-5-Methyl-2-oxo-2-(3-phenyl-propyl)-2λ<sup>5</sup>-[1,3,2]dioxaphospholan-4-one

Synonyms:(S)-5-Methyl-2-oxo-2-(3-phenyl-propyl)-2λ⁵-[1,3,2]dioxaphospholan-4-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-5-Methyl-2-oxo-2-(3-phenyl-propyl)-2λ⁵-[1,3,2]dioxaphospholan-4-one

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Technology Process of (S)-5-Methyl-2-oxo-2-(3-phenyl-propyl)-2λ⁵-[1,3,2]dioxaphospholan-4-one

There total 3 articles about (S)-5-Methyl-2-oxo-2-(3-phenyl-propyl)-2λ⁵-[1,3,2]dioxaphospholan-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 152830-21-2
(2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid

: 1025941-45-0
(S)-5-Methyl-2-oxo-2-(3-phenyl-propyl)-2λ⁵-[1,3,2]dioxaphospholan-4-one

Guidance literature:: With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/jm00030a008

Reference yield:

: 152830-13-2
(2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid benzyl ester

: 1025941-45-0
(S)-5-Methyl-2-oxo-2-(3-phenyl-propyl)-2λ⁵-[1,3,2]dioxaphospholan-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / 1 N LiOH / dioxane / 1 h / Ambient temperature

2: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 0 °C

With lithium hydroxide; 1,1'-carbonyldiimidazole; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/jm00030a008

Reference yield:

: (S)-2-(3-Phenyl-propylphosphinoyloxy)-propionic acid benzyl ester

: 1025941-45-0
(S)-5-Methyl-2-oxo-2-(3-phenyl-propyl)-2λ⁵-[1,3,2]dioxaphospholan-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: NaIO₄ / dioxane; H₂O / 3 h / Ambient temperature

2: 97 percent / 1 N LiOH / dioxane / 1 h / Ambient temperature

3: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 0 °C

With lithium hydroxide; sodium periodate; 1,1'-carbonyldiimidazole; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jm00030a008