Carbamic acid, [(1S)-1-(hydroxymethyl)-4-pentenyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S)-1-(hydroxymethyl)-4-pentenyl]-, 1,1-dimethylethyl ester
CAS No.:225779-17-9
Molecular Formula:C₁₁H₂₁NO₃
Molecular Weight:215.293
Hs Code.:
Mol file:225779-17-9.mol

Synonyms:Carbamicacid, [(1S)-1-(hydroxymethyl)-4-pentenyl]-, 1,1-dimethylethyl ester (9CI);(S)-(1-Hydroxymethylpent-4-enyl)carbamic acid tert-butyl ester

Suppliers and Price of Carbamic acid, [(1S)-1-(hydroxymethyl)-4-pentenyl]-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Carbamic acid, [(1S)-1-(hydroxymethyl)-4-pentenyl]-, 1,1-dimethylethyl ester

Chemical Property:

PSA：58.56000
LogP:2.22910

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Carbamic acid, [(1S)-1-(hydroxymethyl)-4-pentenyl]-, 1,1-dimethylethyl ester

There total 4 articles about Carbamic acid, [(1S)-1-(hydroxymethyl)-4-pentenyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 92136-57-7
(S)-2-tert-butoxycarbonylamino-hex-5-enoic acid methyl ester

: 225779-17-9
tert-butyl N-[(1S)-1-(hydroxymethyl)pent-4-enyl]carbamate

Guidance literature:: With lithium borohydride; In tetrahydrofuran; at 20 ℃; for 18h; Inert atmosphere;

Reference yield:

: 93267-04-0,170848-34-7,889670-02-4
N-(tert-butoxycarbonyl)-L-3-iodoalanine methyl ester

: 225779-17-9
tert-butyl N-[(1S)-1-(hydroxymethyl)pent-4-enyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: zinc; iodine / N,N-dimethyl-formamide / 2 h / 0 - 25 °C

2: N,N-dimethyl-formamide / 16 h / -15 - 20 °C / Inert atmosphere

3: lithium borohydride / tetrahydrofuran / 5 h / 20 °C

With lithium borohydride; iodine; zinc; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: (R)-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)zinc(II)iodide

: 225779-17-9
tert-butyl N-[(1S)-1-(hydroxymethyl)pent-4-enyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 16 h / -15 - 20 °C / Inert atmosphere

2: lithium borohydride / tetrahydrofuran / 5 h / 20 °C

With lithium borohydride; In tetrahydrofuran; N,N-dimethyl-formamide;