8-(3-ethoxycarbonylphenyl)-(3',5'-bis-O-(6-azidopentanoyl))-2'-deoxyguanosine

Base Information

Chemical Name:8-(3-ethoxycarbonylphenyl)-(3',5'-bis-O-(6-azidopentanoyl))-2'-deoxyguanosine
CAS No.:1426244-68-9
Molecular Formula:C₂₉H₃₅N₁₁O₈
Molecular Weight:665.666
Hs Code.:

Synonyms:8-(3-ethoxycarbonylphenyl)-(3',5'-bis-O-(6-azidopentanoyl))-2'-deoxyguanosine

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Chemical Property of 8-(3-ethoxycarbonylphenyl)-(3',5'-bis-O-(6-azidopentanoyl))-2'-deoxyguanosine

Chemical Property:

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Technology Process of 8-(3-ethoxycarbonylphenyl)-(3',5'-bis-O-(6-azidopentanoyl))-2'-deoxyguanosine

There total 3 articles about 8-(3-ethoxycarbonylphenyl)-(3',5'-bis-O-(6-azidopentanoyl))-2'-deoxyguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1426244-66-7
8-(3-ethoxycarbonylphenyl)-(3',5'-bis-O-(6-bromopentanoyl))-2'-deoxyguanosine

: 1426244-68-9
8-(3-ethoxycarbonylphenyl)-(3',5'-bis-O-(6-azidopentanoyl))-2'-deoxyguanosine

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; for 8h;
DOI:10.1021/ja401373h

Reference yield:

: 2067-33-6
5-bromopentanoic acid

: 1426244-68-9
8-(3-ethoxycarbonylphenyl)-(3',5'-bis-O-(6-azidopentanoyl))-2'-deoxyguanosine

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate / N,N-dimethyl-formamide

2: sodium azide / N,N-dimethyl-formamide / 8 h / 80 °C

With sodium azide; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In N,N-dimethyl-formamide;
DOI:10.1021/ja401373h

Reference yield:

: 1130633-92-9
8-(3-ethoxycarbonylphenyl)-2'-deoxyguanosine

: 1426244-68-9
8-(3-ethoxycarbonylphenyl)-(3',5'-bis-O-(6-azidopentanoyl))-2'-deoxyguanosine

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate / N,N-dimethyl-formamide

2: sodium azide / N,N-dimethyl-formamide / 8 h / 80 °C

With sodium azide; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In N,N-dimethyl-formamide;
DOI:10.1021/ja401373h