Technology Process of C14H9(3)HO3
There total 6 articles about C14H9(3)HO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 79 percent / 2-methyl-2-butene; NaH2PO4; NaOCl2 / 2-methyl-propan-2-ol; tetrahydrofuran; H2O / 18 h
2: tritium gas / dimethylformamide
With
sodium dihydrogenphosphate; tritium; 2-methyl-but-2-ene;
In
tetrahydrofuran; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ol0520166
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 77 percent / NaHCO3; Dess-Martin periodinane / CH2Cl2 / 5 h
2: 79 percent / 2-methyl-2-butene; NaH2PO4; NaOCl2 / 2-methyl-propan-2-ol; tetrahydrofuran; H2O / 18 h
3: tritium gas / dimethylformamide
With
sodium dihydrogenphosphate; tritium; 2-methyl-but-2-ene; sodium hydrogencarbonate; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
1: Dess-Martin oxidation;
DOI:10.1021/ol0520166