(2'S)-1-benzoxy-3-<2-(benzoxymethoxy)-1-propyl>-5-bromo-2,6,8-trimethoxynaphthalene

Base Information

Chemical Name:(2'S)-1-benzoxy-3-<2-(benzoxymethoxy)-1-propyl>-5-bromo-2,6,8-trimethoxynaphthalene
CAS No.:159147-22-5
Molecular Formula:C₃₁H₃₃BrO₆
Molecular Weight:581.503
Hs Code.:

Synonyms:(2'S)-1-benzoxy-3-<2-(benzoxymethoxy)-1-propyl>-5-bromo-2,6,8-trimethoxynaphthalene

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Chemical Property of (2'S)-1-benzoxy-3-<2-(benzoxymethoxy)-1-propyl>-5-bromo-2,6,8-trimethoxynaphthalene

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Technology Process of (2'S)-1-benzoxy-3-<2-(benzoxymethoxy)-1-propyl>-5-bromo-2,6,8-trimethoxynaphthalene

There total 7 articles about (2'S)-1-benzoxy-3-<2-(benzoxymethoxy)-1-propyl>-5-bromo-2,6,8-trimethoxynaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 171013-21-1
(2'S)-1-benzoxy-3-<2-(benzoxymethoxy)-1-propyl>-2,6,8-trimethoxynaphthalene

: 159147-22-5
(2'S)-1-benzoxy-3-<2-(benzoxymethoxy)-1-propyl>-5-bromo-2,6,8-trimethoxynaphthalene

Guidance literature:: With N-Bromosuccinimide; at 0 ℃;
DOI:10.1021/ja00098a043

Reference yield:

: 100-39-0
benzyl bromide

: 159147-22-5
(2'S)-1-benzoxy-3-<2-(benzoxymethoxy)-1-propyl>-5-bromo-2,6,8-trimethoxynaphthalene

Guidance literature:: Multi-step reaction with 6 steps

1: 73 percent / n-Bu₄NI

2: LiAlH₄

3: tetrahydrofuran / -78 °C

4: tetrahydrofuran / 67 °C

5: n-Bu₃SnH / toluene / 110 °C

6: NBS / 0 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; toluene;
DOI:10.1021/ja00098a043

Reference yield:

: 132019-89-7
methyl 2,6,8-trimethoxy-1-hydroxynaphthalene-3-carboxylate

: 159147-22-5
(2'S)-1-benzoxy-3-<2-(benzoxymethoxy)-1-propyl>-5-bromo-2,6,8-trimethoxynaphthalene

Guidance literature:: Multi-step reaction with 6 steps

1: 73 percent / n-Bu₄NI

2: LiAlH₄

3: tetrahydrofuran / -78 °C

4: tetrahydrofuran / 67 °C

5: n-Bu₃SnH / toluene / 110 °C

6: NBS / 0 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; toluene;
DOI:10.1021/ja00098a043