C₂₉H₃₀N₂O₆

Base Information

Chemical Name:C₂₉H₃₀N₂O₆
CAS No.:1399266-42-2
Molecular Formula:C₂₉H₃₀N₂O₆
Molecular Weight:502.567
Hs Code.:

C<sub>29</sub>H<sub>30</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₉H₃₀N₂O₆

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Chemical Property of C₂₉H₃₀N₂O₆

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Technology Process of C₂₉H₃₀N₂O₆

There total 9 articles about C₂₉H₃₀N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1399266-39-7
C₂₄H₂₂N₂O₄

: 1399266-42-2
C₂₉H₃₀N₂O₆

Guidance literature:: In tetrahydrofuran; acetonitrile; at 60 ℃; for 68h; Inert atmosphere;
DOI:10.1039/c2ob26077h

Reference yield:

: 65-49-6
4-Aminosalicylic acid

: 1399266-42-2
C₂₉H₃₀N₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: sulfuric acid / 22 °C

2.1: acetic acid / 22 h / 118 °C / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 22 °C / Inert atmosphere

4.1: potassium hydroxide; water / methanol / 18.5 h / 22 °C

5.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3.5 h / 22 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 22 °C / Inert atmosphere

7.1: diethylamino-sulfur trifluoride / dichloromethane / 5 h / -78 °C / Inert atmosphere

7.2: -78 - 22 °C

8.1: tetrahydrofuran / 0.25 h / 0 °C

8.2: 3 h / 0 - 22 °C

9.1: tetrahydrofuran; acetonitrile / 68 h / 60 °C / Inert atmosphere

With oxalyl dichloride; diethylamino-sulfur trifluoride; sulfuric acid; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2ob26077h

Reference yield:

: 4136-97-4
methyl 4-aminosalicylate

: 1399266-42-2
C₂₉H₃₀N₂O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: acetic acid / 22 h / 118 °C / Inert atmosphere

2.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 22 °C / Inert atmosphere

3.1: potassium hydroxide; water / methanol / 18.5 h / 22 °C

4.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3.5 h / 22 °C / Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 22 °C / Inert atmosphere

6.1: diethylamino-sulfur trifluoride / dichloromethane / 5 h / -78 °C / Inert atmosphere

6.2: -78 - 22 °C

7.1: tetrahydrofuran / 0.25 h / 0 °C

7.2: 3 h / 0 - 22 °C

8.1: tetrahydrofuran; acetonitrile / 68 h / 60 °C / Inert atmosphere

With oxalyl dichloride; diethylamino-sulfur trifluoride; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2ob26077h