(R)-3-([(R)-2-amino-2-oxo-1-phenylethyl]amino)-3-phenylpropionic acid ethyl ester hydrochloride

Base Information

Chemical Name:(R)-3-([(R)-2-amino-2-oxo-1-phenylethyl]amino)-3-phenylpropionic acid ethyl ester hydrochloride
CAS No.:893395-89-6
Molecular Formula:C₁₉H₂₂N₂O₃*ClH
Molecular Weight:362.856
Hs Code.:

Synonyms:(R)-3-([(R)-2-amino-2-oxo-1-phenylethyl]amino)-3-phenylpropionic acid ethyl ester hydrochloride

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Chemical Property of (R)-3-([(R)-2-amino-2-oxo-1-phenylethyl]amino)-3-phenylpropionic acid ethyl ester hydrochloride

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Technology Process of (R)-3-([(R)-2-amino-2-oxo-1-phenylethyl]amino)-3-phenylpropionic acid ethyl ester hydrochloride

There total 1 articles about (R)-3-([(R)-2-amino-2-oxo-1-phenylethyl]amino)-3-phenylpropionic acid ethyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 105-36-2
ethyl bromoacetate

: 741681-30-1
(R)-2-[(phenylmethylene)amino]-2-phenylacetamide

: 893395-89-6
(R)-3-([(R)-2-amino-2-oxo-1-phenylethyl]amino)-3-phenylpropionic acid ethyl ester hydrochloride

Guidance literature:: ethyl bromoacetate; (R)-2-[(phenylmethylene)amino]-2-phenylacetamide; With zinc; In dichloromethane; at 42 ℃; for 5.33333h; Heating / reflux;

With hydrogenchloride; water; In dichloromethane; for 15h; Product distribution / selectivity;

Reference yield: 54.0%

: 893395-89-6
(R)-3-([(R)-2-amino-2-oxo-1-phenylethyl]amino)-3-phenylpropionic acid ethyl ester hydrochloride

: 3082-68-6
(R)-3-amino-3-phenylpropionic acid ethyl ester

Guidance literature:: (R)-3-([(R)-2-amino-2-oxo-1-phenylethyl]amino)-3-phenylpropionic acid ethyl ester hydrochloride; With triethylamine; trichlorophosphate; In tetrahydrofuran; at 0 - 20 ℃; for 6h; Heating / reflux;

With hydroxylamine hydrochloride; In tetrahydrofuran; water; at 20 ℃; for 16h;

With hydrogenchloride; sodium hydroxide; more than 3 stages; Product distribution / selectivity;