potassium {[5-(3-fluorophenyl)-3-hydroxypyridine-2-carbonyl]amino}acetate

Base Information

Chemical Name:potassium {[5-(3-fluorophenyl)-3-hydroxypyridine-2-carbonyl]amino}acetate
CAS No.:1415796-79-0
Molecular Formula:C₁₄H₁₀FN₂O₄*K
Molecular Weight:328.341
Hs Code.:

Synonyms:potassium {[5-(3-fluorophenyl)-3-hydroxypyridine-2-carbonyl]amino}acetate

Suppliers and Price of potassium {[5-(3-fluorophenyl)-3-hydroxypyridine-2-carbonyl]amino}acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of potassium {[5-(3-fluorophenyl)-3-hydroxypyridine-2-carbonyl]amino}acetate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of potassium {[5-(3-fluorophenyl)-3-hydroxypyridine-2-carbonyl]amino}acetate

There total 8 articles about potassium {[5-(3-fluorophenyl)-3-hydroxypyridine-2-carbonyl]amino}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85331-33-5
2-Cyano-3,5-dichloropyridine

: 1415796-79-0
potassium {[5-(3-fluorophenyl)-3-hydroxypyridine-2-carbonyl]amino}acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide; water / 20 - 53 °C / Inert atmosphere; Large scale

2.1: methanol / 68 °C / Large scale

3.1: hydrogenchloride; water / 67 - 110 °C / Large scale

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 6 °C / Large scale

5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 19 - 25 °C / Large scale

5.2: 0 - 25 °C / Large scale

6.1: hydrogenchloride / water; tetrahydrofuran / 19 - 25 °C / pH Ca_. 2 / Large scale

7.1: potassium hydroxide / water; methanol / 50 °C

With hydrogenchloride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1007377-55-0
{[5-(3-fluorophenyl)-3-hydroxy-pyridine-2-carbonyl]amino}acetic acid

: 1415796-79-0
potassium {[5-(3-fluorophenyl)-3-hydroxypyridine-2-carbonyl]amino}acetate

Guidance literature:: With potassium hydroxide; In methanol; water; at 50 ℃; Solvent;

Reference yield:

: 1415796-65-4
5-(3-fluorophenyl)-3-chloro-2-cyanopyridine

: 1415796-79-0
potassium {[5-(3-fluorophenyl)-3-hydroxypyridine-2-carbonyl]amino}acetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: methanol / 68 °C / Large scale

2.1: hydrogenchloride; water / 67 - 110 °C / Large scale

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 6 °C / Large scale

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 19 - 25 °C / Large scale

4.2: 0 - 25 °C / Large scale

5.1: hydrogenchloride / water; tetrahydrofuran / 19 - 25 °C / pH Ca_. 2 / Large scale

6.1: potassium hydroxide / water; methanol / 50 °C

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In tetrahydrofuran; methanol; water;