(2R,4S,6R)-2-[2-(benzyloxy)ethyl]-6-([(tert-butyl)dimethylsilyl]oxymethyl)tetrahydro-2H-4-pyranol

Base Information

Chemical Name:(2R,4S,6R)-2-[2-(benzyloxy)ethyl]-6-([(tert-butyl)dimethylsilyl]oxymethyl)tetrahydro-2H-4-pyranol
CAS No.:1263875-93-9
Molecular Formula:C₂₁H₃₆O₄Si
Molecular Weight:380.6
Hs Code.:

Synonyms:(2R,4S,6R)-2-[2-(benzyloxy)ethyl]-6-([(tert-butyl)dimethylsilyl]oxymethyl)tetrahydro-2H-4-pyranol

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Chemical Property of (2R,4S,6R)-2-[2-(benzyloxy)ethyl]-6-([(tert-butyl)dimethylsilyl]oxymethyl)tetrahydro-2H-4-pyranol

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Technology Process of (2R,4S,6R)-2-[2-(benzyloxy)ethyl]-6-([(tert-butyl)dimethylsilyl]oxymethyl)tetrahydro-2H-4-pyranol

There total 1 articles about (2R,4S,6R)-2-[2-(benzyloxy)ethyl]-6-([(tert-butyl)dimethylsilyl]oxymethyl)tetrahydro-2H-4-pyranol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1263875-92-8
(2R,4S,6R)-2-[2-(benzyloxy)ethyl]-6-(hydroxymethyl)tetrahydro-2H-4-pyranol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1263875-93-9
(2R,4S,6R)-2-[2-(benzyloxy)ethyl]-6-([(tert-butyl)dimethylsilyl]oxymethyl)tetrahydro-2H-4-pyranol

Guidance literature:: (2R,4S,6R)-2-[2-(benzyloxy)ethyl]-6-(hydroxymethyl)tetrahydro-2H-4-pyranol; With 1H-imidazole; In dichloromethane; at 0 ℃; for 0.25h;

tert-butyldimethylsilyl chloride; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1055/s-0030-1258253

Reference yield: 75.0%

: 1263875-93-9
(2R,4S,6R)-2-[2-(benzyloxy)ethyl]-6-([(tert-butyl)dimethylsilyl]oxymethyl)tetrahydro-2H-4-pyranol

: 1263875-94-0
(2R,4R,6R)-2-[2-(benzyloxy)ethyl]-6-([(tert-butyl)dimethylsilyl]oxymethyl)tetrahydro-2H-4-pyranol

Guidance literature:: (2R,4S,6R)-2-[2-(benzyloxy)ethyl]-6-([(tert-butyl)dimethylsilyl]oxymethyl)tetrahydro-2H-4-pyranol; With triphenylphosphine; diethylazodicarboxylate; 4-nitro-benzoic acid; In toluene; at -78 - -20 ℃;

With potassium carbonate; In methanol; toluene; at 20 ℃; for 1h;
DOI:10.1055/s-0030-1258253