16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

Base Information

Chemical Name:16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one
CAS No.:1384487-71-1
Molecular Formula:C₂₃H₁₇N₅O
Molecular Weight:379.421
Hs Code.:

Synonyms:16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

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Chemical Property of 16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

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Technology Process of 16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

There total 4 articles about 16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 16714-27-5
(2-azidophenyl)(phenyl)methanone

: 4943-83-3
2-amino-N-(prop-2-yn-1-yl)benzamide

: 1384487-71-1
16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

Guidance literature:: With iodine; In methanol; at 50 ℃;
DOI:10.1021/ol301592z

Reference yield:

: C₁₁H₁₀N₂O₃

: 1384487-71-1
16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water

2: iodine / methanol / 50 °C

With iodine; sodium hydroxide; In methanol; water;
DOI:10.1021/ol301592z

Reference yield:

: 118-48-9
isatoic anhydride

: 1384487-71-1
16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 10 h / 50 °C

2: sodium hydroxide / water

3: iodine / methanol / 50 °C

With iodine; sodium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol301592z