C₂₉H₃₆FN₃O₃Si

Base Information

Chemical Name:C₂₉H₃₆FN₃O₃Si
CAS No.:1196037-86-1
Molecular Formula:C₂₉H₃₆FN₃O₃Si
Molecular Weight:521.707
Hs Code.:

C<sub>29</sub>H<sub>36</sub>FN<sub>3</sub>O<sub>3</sub>Si

Synonyms:C₂₉H₃₆FN₃O₃Si

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Chemical Property of C₂₉H₃₆FN₃O₃Si

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Technology Process of C₂₉H₃₆FN₃O₃Si

There total 11 articles about C₂₉H₃₆FN₃O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 887510-02-3
(2-(bromomethyl)-4-fluorophenoxy)(tert-butyl)dimethylsilane

: 1029691-23-3
(S)-(7-cyano-1,2,3,4-tetrahydrocyclopenta[b]indol-2-yl)carbamic acid isopropyl ester

: 1196037-86-1
C₂₉H₃₆FN₃O₃Si

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at -40 - 20 ℃; Cooling with dry ice;

Reference yield:

: 930-30-3
cyclopent-2-enone

: 1196037-86-1
C₂₉H₃₆FN₃O₃Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium carbonate / methanol; water / 20 °C

2.1: acetic acid / 5 h / Reflux

3.1: hydrazine hydrate / tetrahydrofuran; water / 22 h / 20 - 55 °C

4.1: sodium hydrogencarbonate / tetrahydrofuran; water / 20 °C

5.1: Chiralcel OJ 8 / Resolution of racemate

6.1: zinc diacetate; zinc / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 18 h / 100 °C

7.1: hydrogenchloride / 1,4-dioxane / 18 h / 20 °C

7.2: 4 h / 20 °C

8.1: caesium carbonate / N,N-dimethyl-formamide / -40 - 20 °C / Cooling with dry ice

With hydrogenchloride; zinc diacetate; sodium hydrogencarbonate; sodium carbonate; caesium carbonate; hydrazine hydrate; acetic acid; zinc; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1196037-59-8
((R,S)-7-Bromo-1,2,3,4-tetrahydro-cyclopenta[b]indol-2-yl)-carbamic acid tert-butyl ester

: 1196037-86-1
C₂₉H₃₆FN₃O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: Chiralcel OJ 8 / Resolution of racemate

2.1: zinc diacetate; zinc / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 18 h / 100 °C

3.1: hydrogenchloride / 1,4-dioxane / 18 h / 20 °C

3.2: 4 h / 20 °C

4.1: caesium carbonate / N,N-dimethyl-formamide / -40 - 20 °C / Cooling with dry ice

With hydrogenchloride; zinc diacetate; caesium carbonate; zinc; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; N,N-dimethyl-formamide;