15-methoxy-16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

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Chemical Name:15-methoxy-16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one
CAS No.:1384487-73-3
Molecular Formula:C₂₄H₁₉N₅O₂
Molecular Weight:409.447
Hs Code.:

Synonyms:15-methoxy-16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

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Chemical Property of 15-methoxy-16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

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Technology Process of 15-methoxy-16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

There total 4 articles about 15-methoxy-16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 16714-27-5
(2-azidophenyl)(phenyl)methanone

: 1384487-61-9
2-amino-3-methoxy-N-(prop-2-yn-1-yl)benzamide

: 1384487-73-3
15-methoxy-16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

Guidance literature:: With iodine; In methanol; at 50 ℃;
DOI:10.1021/ol301592z

Reference yield:

: C₁₁H₁₁N₃O₂

: 1384487-73-3
15-methoxy-16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 20 °C

2: iodine / methanol / 50 °C

With iodine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ol301592z

Reference yield:

: 3177-80-8
2-amino-3-methoxybenzoic acid

: 1384487-73-3
15-methoxy-16a-phenyl-16,16a-dihydrobenzo[5,6][1,2,3]triazolo[5',1':3,4][1,4]diazepino[7,1-b]quinazolin-11(9H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 12 h / 40 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 20 °C

3: iodine / methanol / 50 °C

With iodine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ol301592z