1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,7-dihydro-2H-1,3-diazepine-2,4(3H)-dione

Base Information

• Chemical Name: 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,7-dihydro-2H-1,3-diazepine-2,4(3H)-dione
• CAS No.: 107711-26-2
• Molecular Formula: C₃₁H₂₆N₂O₉
• Molecular Weight: 570.555

Synonyms:1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,7-dihydro-2H-1,3-diazepine-2,4(3H)-dione

Chemical Property of 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,7-dihydro-2H-1,3-diazepine-2,4(3H)-dione

Chemical Property:

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Technology Process of 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,7-dihydro-2H-1,3-diazepine-2,4(3H)-dione

There total 2 articles about 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,7-dihydro-2H-1,3-diazepine-2,4(3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2-one (77249-70-8) → 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,7-dihydro-2H-1,3-diazepine-2,4(3H)-dione (107711-26-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 33 percent / toluene / 1 h / Heating

2: 1.) m-chloroperbenzoic acid, 2.) diethylamine / 1.) chloroform, RT, 15 min, 2.) reflux

With diethylamine; 3-chloro-benzenecarboperoxoic acid; In toluene;

DOI:10.1021/jo00386a015

Reference yield:

C37H32N2O9Se (107711-23-9,107711-24-0) → 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,7-dihydro-2H-1,3-diazepine-2,4(3H)-dione (107711-26-2)

Guidance literature:

With diethylamine; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1.) chloroform, RT, 15 min, 2.) reflux;

DOI:10.1021/jo00386a015

Reference yield: 85.0%

1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,7-dihydro-2H-1,3-diazepine-2,4(3H)-dione (107711-26-2) → 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4-thioxo-1,3,4,7-tetrahydro-2H-1,3-diazepin-2-one (107711-27-3)

Guidance literature:

With Lawessons reagent; In benzene; for 4h; Heating;

DOI:10.1021/jo00386a015

upstream raw materials:

C₃₇H₃₂N₂O₉Se

1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2-one

Downstream raw materials:

1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4-thioxo-1,3,4,7-tetrahydro-2H-1,3-diazepin-2-one

1-β-D-ribofuranosyl-4-amino-1,7-dihydro-2H-1,3-diazepine-2-one

C₃₂H₂₈N₂O₈S

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