2-bromo-N-(4-(cyclopropyl(ethyl)carbamoyl)phenyl)-N-(2,4-dimethoxybenzyl)cyclohept-1-ene-1-carboxamide

Base Information

Chemical Name:2-bromo-N-(4-(cyclopropyl(ethyl)carbamoyl)phenyl)-N-(2,4-dimethoxybenzyl)cyclohept-1-ene-1-carboxamide
CAS No.:1616681-10-7
Molecular Formula:C₂₉H₃₅BrN₂O₄
Molecular Weight:555.512
Hs Code.:

Synonyms:2-bromo-N-(4-(cyclopropyl(ethyl)carbamoyl)phenyl)-N-(2,4-dimethoxybenzyl)cyclohept-1-ene-1-carboxamide

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Chemical Property of 2-bromo-N-(4-(cyclopropyl(ethyl)carbamoyl)phenyl)-N-(2,4-dimethoxybenzyl)cyclohept-1-ene-1-carboxamide

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Technology Process of 2-bromo-N-(4-(cyclopropyl(ethyl)carbamoyl)phenyl)-N-(2,4-dimethoxybenzyl)cyclohept-1-ene-1-carboxamide

There total 6 articles about 2-bromo-N-(4-(cyclopropyl(ethyl)carbamoyl)phenyl)-N-(2,4-dimethoxybenzyl)cyclohept-1-ene-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 90002-61-2
2-bromo-1-cycloheptene-1-carboxylic acid

: 1616681-08-3
N-cyclopropyl-N-ethyl-4-((2,4-dimethoxybenzyl)amino)benzamide

: 1616681-10-7
2-bromo-N-(4-(cyclopropyl(ethyl)carbamoyl)phenyl)-N-(2,4-dimethoxybenzyl)cyclohept-1-ene-1-carboxamide

Guidance literature:: N-cyclopropyl-N-ethyl-4-((2,4-dimethoxybenzyl)amino)benzamide; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 0.166667h;

2-bromo-1-cycloheptene-1-carboxylic acid; With dmap; In dichloromethane; at 60 ℃; for 2h;
DOI:10.1016/j.bmc.2014.05.022

Reference yield:

: 85236-13-1
2-bromocyclohept-1-ene-1-carbaldehyde

: 1616681-10-7
2-bromo-N-(4-(cyclopropyl(ethyl)carbamoyl)phenyl)-N-(2,4-dimethoxybenzyl)cyclohept-1-ene-1-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium dihydrogenphosphate; dihydrogen peroxide; sodium chlorite / water; acetonitrile / 20 °C

2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / 20 °C

2.2: 2 h / 60 °C

With sodium chlorite; sodium dihydrogenphosphate; oxalyl dichloride; dihydrogen peroxide; N,N-dimethyl-formamide; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmc.2014.05.022

Reference yield:

: 502-42-1
cycloheptanone

: 1616681-10-7
2-bromo-N-(4-(cyclopropyl(ethyl)carbamoyl)phenyl)-N-(2,4-dimethoxybenzyl)cyclohept-1-ene-1-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: phosphorus tribromide / chloroform / 4 h / 0 - 20 °C / Reflux

2.1: sodium dihydrogenphosphate; dihydrogen peroxide; sodium chlorite / water; acetonitrile / 20 °C

3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / 20 °C

3.2: 2 h / 60 °C

With sodium chlorite; sodium dihydrogenphosphate; oxalyl dichloride; dihydrogen peroxide; phosphorus tribromide; N,N-dimethyl-formamide; In dichloromethane; chloroform; water; acetonitrile;
DOI:10.1016/j.bmc.2014.05.022