6-p-anisyl-2-(p-anisylamino)-3[(4H)-p-anisyliminobis(2-(m-tolylazo)pyridine)]-9-methoxyphenazineosmium(II) bromide

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Chemical Name:6-p-anisyl-2-(p-anisylamino)-3[(4H)-p-anisyliminobis(2-(m-tolylazo)pyridine)]-9-methoxyphenazineosmium(II) bromide
CAS No.:306970-36-5
Molecular Formula:Br*C₅₈H₅₁N₁₀O₄Os
Molecular Weight:1222.21
Hs Code.:

Synonyms:6-p-anisyl-2-(p-anisylamino)-3[(4H)-p-anisyliminobis(2-(m-tolylazo)pyridine)]-9-methoxyphenazineosmium(II) bromide

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Chemical Property of 6-p-anisyl-2-(p-anisylamino)-3[(4H)-p-anisyliminobis(2-(m-tolylazo)pyridine)]-9-methoxyphenazineosmium(II) bromide

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Technology Process of 6-p-anisyl-2-(p-anisylamino)-3[(4H)-p-anisyliminobis(2-(m-tolylazo)pyridine)]-9-methoxyphenazineosmium(II) bromide

There total 1 articles about 6-p-anisyl-2-(p-anisylamino)-3[(4H)-p-anisyliminobis(2-(m-tolylazo)pyridine)]-9-methoxyphenazineosmium(II) bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 87172-03-0,144016-85-3,87114-22-5
Os(2-(m-tolylazo)-pyridine)2Br₂

: 306970-26-3
7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine

: 306970-36-5
6-p-anisyl-2-(p-anisylamino)-3[(4H)-p-anisyliminobis(2-(m-tolylazo)pyridine)]-9-methoxyphenazineosmium(II) bromide

Guidance literature:: With sodium carbonate; In 2-methoxy-ethanol; under N2, molar ratio was 1:1, reflux for 5 h, Na2CO3 was used as base; soln. was evapd., solid was dissolved in CHCl3, chromy. on silica gel (CH3CN/CH2Cl2=1:12 and 1:6), solvent was evapd. from last fraction, recrystn. from CH2Cl2/hexane, elem. anal.;
DOI:10.1002/1099-0682(200009)2000:9<1961::aid-ejic1961>3.3.co;2-2