7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine

Base Information

Chemical Name:7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine
CAS No.:306970-26-3
Molecular Formula:C₃₄H₃₀N₄O₄
Molecular Weight:558.637
Hs Code.:

Synonyms:7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine

Suppliers and Price of 7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine

There total 1 articles about 7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 104-94-9
4-methoxy-aniline

: 306970-26-3
7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine

Guidance literature:: With perchloric acid; oxygen; at 100 ℃;
DOI:10.1021/jo3019126

Reference yield: 80.0%

: 87172-03-0,144016-85-3,87114-22-5
Os(2-(m-tolylazo)-pyridine)2Br₂

: 306970-26-3
7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine

: 306970-36-5
6-p-anisyl-2-(p-anisylamino)-3[(4H)-p-anisyliminobis(2-(m-tolylazo)pyridine)]-9-methoxyphenazineosmium(II) bromide

Guidance literature:: With sodium carbonate; In 2-methoxy-ethanol; under N2, molar ratio was 1:1, reflux for 5 h, Na2CO3 was used as base; soln. was evapd., solid was dissolved in CHCl3, chromy. on silica gel (CH3CN/CH2Cl2=1:12 and 1:6), solvent was evapd. from last fraction, recrystn. from CH2Cl2/hexane, elem. anal.;
DOI:10.1002/1099-0682(200009)2000:9<1961::aid-ejic1961>3.3.co;2-2

Reference yield: 10.0%

: 67-56-1
methanol

: cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate

: 306970-26-3
7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine

: 14797-73-0,1059018-91-5
perchlorate^(1-)

: 957110-69-9
[Ru(II)(2,2'-bipyridine)2(6-p-anisyl-2-(p-anisylamino)-3(4H)-p-anisylimine-9-methoxyphenazine(-H))]ClO₄

: [Ru(II)(2,2'-bipyridine)2(7-methoxy-5-(4-methoxyphenylimino)-3,5-dihydro-2H-phenazin-1-one))][ClO₄]2

: [Ru₂(2,2'-bipyridine)4(7,8'-dimethoxy-5,10'-bis(4-methoxyphenyl)-2,3'-bis(4-methoxyphenylamino)-3,2'-bis(4-methoxyphenylimine)-..

Guidance literature:: With AgNO₃; triethyl amine; air; In methanol; byproducts: AgCl; mixt. of Ru(bpy)2Cl2*2H2O (0.125 mmol) and AgNO3 (0.25 mmol) in MeOH refluxed for 2 h, filtered, phenazine deriv. (0.125 mmol) and two drops of Et3N added to filtrate, mixt. refluxed for 6 h; concd., poured into Et2O, ppt. sepd., mixt. sepd. by repeated preparative TLC (Al2O3, CHCl3 and CHCl3/CH3CN), recrystn. (CH2Cl2/hexane); elem. anal.;
DOI:10.1002/ejic.200600864