cyano-(1-methyl-2-morpholin-4-yl-2-phenyl-vinylimino)-acetic acid methyl ester

Base Information

• Chemical Name: cyano-(1-methyl-2-morpholin-4-yl-2-phenyl-vinylimino)-acetic acid methyl ester
• CAS No.: 56176-95-5
• Molecular Formula: C₁₇H₁₉N₃O₃
• Molecular Weight: 313.356
• Mol file: 56176-95-5.mol

Synonyms:cyano-(1-methyl-2-morpholin-4-yl-2-phenyl-vinylimino)-acetic acid methyl ester

Chemical Property of cyano-(1-methyl-2-morpholin-4-yl-2-phenyl-vinylimino)-acetic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyano-(1-methyl-2-morpholin-4-yl-2-phenyl-vinylimino)-acetic acid methyl ester

There total 2 articles about cyano-(1-methyl-2-morpholin-4-yl-2-phenyl-vinylimino)-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyano-(toluene-4-sulfonyloxyimino)-acetic acid methyl ester (49845-22-9) + [E]-1-morpholino-1-phenyl-1-propene (30085-70-2) → cyano-(1-methyl-2-morpholin-4-yl-2-phenyl-vinylimino)-acetic acid methyl ester (56176-95-5)

Guidance literature:

With triethylamine; In dichloromethane; at 25 ℃; Rate constant;

DOI:10.1016/0040-4020(75)80069-X

Reference yield:

→ cyano-(1-methyl-2-morpholin-4-yl-2-phenyl-vinylimino)-acetic acid methyl ester (56176-95-5)

Guidance literature:

Cyanester 1c,Enamin 4k;

DOI:10.1016/0040-4020(75)80069-X

Reference yield: 92.0%

cyano-(1-methyl-2-morpholin-4-yl-2-phenyl-vinylimino)-acetic acid methyl ester (56176-95-5) + potassium cyanide (151-50-8) → amino-4-methyl-2-morpholino-3-phenyl-3-3H-pyrrolecarbonitrile-5

Guidance literature:

In methanol; at 20 ℃; for 0.5h;

DOI:10.1002/hlca.19870700123

upstream raw materials:

cyano-(toluene-4-sulfonyloxyimino)-acetic acid methyl ester

[E]-1-morpholino-1-phenyl-1-propene

Downstream raw materials:

methyl-phenylglyoxal disemicarbazone

1-phenyl-1,2-propanedione dioxime

1-Phenyl-1,2-propandion-bis(hydrazon)