octyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Base Information

Chemical Name:octyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside
CAS No.:857633-32-0
Molecular Formula:C₃₅H₄₀O₉
Molecular Weight:604.697
Hs Code.:

Synonyms:octyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside

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Chemical Property of octyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside

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Technology Process of octyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside

There total 6 articles about octyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 857633-31-9
octyl 2,3,4-tri-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-α-D-mannopyranoside

: 857633-32-0
octyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: With methanol; acetyl chloride; In diethyl ether; at 20 ℃; for 96h;
DOI:10.1039/b503919c

Reference yield:

: 950602-63-8
octyl 6-O-(tert-butyldiphenylsilyl)-α-D-mannopyranoside

: 857633-32-0
octyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 3.80 g / DMAP; pyridine / 18 h / 20 °C

2: 58 percent / acetyl chloride; methanol / diethyl ether / 96 h / 20 °C

With pyridine; methanol; dmap; acetyl chloride; In diethyl ether;
DOI:10.1039/b503919c

Reference yield:

: 111-87-5
octanol

: 857633-32-0
octyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: SnCl₄; 4 Angstroem molecular sieves / CH₂Cl₂ / 19 h / 20 °C

2: 2.43 g / NaOMe / methanol / 1 h

3: imidazole / dimethylformamide / 3 h / 35 °C

4: 3.80 g / DMAP; pyridine / 18 h / 20 °C

5: 58 percent / acetyl chloride; methanol / diethyl ether / 96 h / 20 °C

With pyridine; 1H-imidazole; methanol; dmap; 4 A molecular sieve; sodium methylate; tin(IV) chloride; acetyl chloride; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b503919c