Z-2-<3,4-dimethoxyphenyl>-1-tert-butyldimethylsilyloxy methyl propenoate

Base Information

• Chemical Name: Z-2-<3,4-dimethoxyphenyl>-1-tert-butyldimethylsilyloxy methyl propenoate
• CAS No.: 232266-92-1
• Molecular Formula: C₁₈H₂₈O₅Si
• Molecular Weight: 352.503

Synonyms:Z-2-<3,4-dimethoxyphenyl>-1-tert-butyldimethylsilyloxy methyl propenoate

Chemical Property of Z-2-<3,4-dimethoxyphenyl>-1-tert-butyldimethylsilyloxy methyl propenoate

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Technology Process of Z-2-<3,4-dimethoxyphenyl>-1-tert-butyldimethylsilyloxy methyl propenoate

There total 1 articles about Z-2-<3,4-dimethoxyphenyl>-1-tert-butyldimethylsilyloxy methyl propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

methyl 2-oxo 3-(3,4-dimethoxyphenyl) propanoate (35271-83-1) + tert-butyldimethylsilyl chloride (18162-48-6) → Z-2-<3,4-dimethoxyphenyl>-1-tert-butyldimethylsilyloxy methyl propenoate (232266-92-1) + 2-(3,4-dimethoxy-benzyl)-3-(3,4-dimethoxy-phenyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-2-carboxylic acid methyl ester

Guidance literature:

With dmap; triethylamine; In dichloromethane;

DOI:10.1016/S0040-4020(99)00317-8

Reference yield: 90.0%

Z-2-<3,4-dimethoxyphenyl>-1-tert-butyldimethylsilyloxy methyl propenoate (232266-92-1) → Z-3-<3,4-dimethoxyphenyl>-2-tert-butyldimethylsilyloxy prop-2-enol

Guidance literature:

With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 0.166667h;

DOI:10.1016/S0040-4020(99)00317-8

Reference yield: 85.0%

Z-2-<3,4-dimethoxyphenyl>-1-tert-butyldimethylsilyloxy methyl propenoate (232266-92-1) → 3-<3,4-dimethoxyphenyl>-2-oxo propanol (78886-14-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; Ambient temperature;

DOI:10.1016/S0040-4020(99)00317-8

upstream raw materials:

methyl 2-oxo 3-(3,4-dimethoxyphenyl) propanoate

tert-butyldimethylsilyl chloride

Downstream raw materials:

Z-2-<3,4-dimethoxyphenyl>-1-tert-butyldimethylsilyloxy ethyl propenoate

3-<3,4-dimethoxyphenyl>-2-oxo propanol

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