3-(3',6-dimethoxy-[1,1'-biphenyl]-3-ylcarboxamido)-6-methoxy-8-methyl-2-oxo-2H-chromen-7-yl acetate

Base Information

Chemical Name:3-(3',6-dimethoxy-[1,1'-biphenyl]-3-ylcarboxamido)-6-methoxy-8-methyl-2-oxo-2H-chromen-7-yl acetate
CAS No.:1160952-38-4
Molecular Formula:C₂₈H₂₅NO₈
Molecular Weight:503.508
Hs Code.:

Synonyms:3-(3',6-dimethoxy-[1,1'-biphenyl]-3-ylcarboxamido)-6-methoxy-8-methyl-2-oxo-2H-chromen-7-yl acetate

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Chemical Property of 3-(3',6-dimethoxy-[1,1'-biphenyl]-3-ylcarboxamido)-6-methoxy-8-methyl-2-oxo-2H-chromen-7-yl acetate

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Technology Process of 3-(3',6-dimethoxy-[1,1'-biphenyl]-3-ylcarboxamido)-6-methoxy-8-methyl-2-oxo-2H-chromen-7-yl acetate

There total 4 articles about 3-(3',6-dimethoxy-[1,1'-biphenyl]-3-ylcarboxamido)-6-methoxy-8-methyl-2-oxo-2H-chromen-7-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1083313-80-7
3',6-dimethoxy-[1,1'-biphenyl]-3-carbonyl chloride

: 1308889-58-8
C₁₃H₁₃NO₅

: 1160952-38-4
3-(3',6-dimethoxy-[1,1'-biphenyl]-3-ylcarboxamido)-6-methoxy-8-methyl-2-oxo-2H-chromen-7-yl acetate

Guidance literature:: With triethylamine; In tetrahydrofuran; for 12h;
DOI:10.1021/jm200148p

Reference yield:

: 1083312-78-0
benzyl 7-hydroxy-6-methoxy-8-methyl-2-oxo-2H-chromen-3-ylcarbamate

: 1160952-38-4
3-(3',6-dimethoxy-[1,1'-biphenyl]-3-ylcarboxamido)-6-methoxy-8-methyl-2-oxo-2H-chromen-7-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 12 h

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 12 h

3: triethylamine / tetrahydrofuran / 12 h

With palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; pyridine;
DOI:10.1021/jm200148p

Reference yield:

: 1083313-05-6
3′,6-dimethoxy-[1,1′-biphenyl]-3-carboxylic acid

: 1160952-38-4
3-(3',6-dimethoxy-[1,1'-biphenyl]-3-ylcarboxamido)-6-methoxy-8-methyl-2-oxo-2H-chromen-7-yl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / tetrahydrofuran

2: triethylamine / tetrahydrofuran / 12 h

With thionyl chloride; triethylamine; In tetrahydrofuran;
DOI:10.1021/jm200148p