C₁₄H₉F₃O

Base Information

Chemical Name:C₁₄H₉F₃O
CAS No.:1188522-84-0
Molecular Formula:C₁₄H₉F₃O
Molecular Weight:250.22
Hs Code.:

C<sub>14</sub>H<sub>9</sub>F<sub>3</sub>O

Synonyms:C₁₄H₉F₃O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₉F₃O

Chemical Property:

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Technology Process of C₁₄H₉F₃O

There total 3 articles about C₁₄H₉F₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1188475-54-8
C₁₀H₁₁F₂NO₂

: 460-00-4
1-Bromo-4-fluorobenzene

: 1188522-84-0
C₁₄H₉F₃O

Guidance literature:: 1-Bromo-4-fluorobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -40 - -10 ℃; for 2h; Inert atmosphere;

C₁₀H₁₁F₂NO₂; In tetrahydrofuran; hexane; at -78 ℃;

Reference yield:

: 4122-56-9
methyl o-formylbenzoate

: 1188522-84-0
C₁₄H₉F₃O

Guidance literature:: Multi-step reaction with 3 steps

1.1: diethylamino-sulfur trifluoride / methanol / dichloromethane / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -40 - -10 °C / Inert atmosphere

3.2: -78 °C

With n-butyllithium; diethylamino-sulfur trifluoride; methanol; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 1018678-48-2
methyl 5-phenyl-2-difluoromethylbenzoate

: 1188522-84-0
C₁₄H₉F₃O

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -40 - -10 °C / Inert atmosphere

2.2: -78 °C

With n-butyllithium; In tetrahydrofuran; hexane;