benzyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-ε-aminohexanoate

Base Information

Chemical Name:benzyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-ε-aminohexanoate
CAS No.:87919-07-1
Molecular Formula:C₆₃H₉₅NO₁₇
Molecular Weight:1138.44
Hs Code.:

Synonyms:benzyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-ε-aminohexanoate

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Chemical Property of benzyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-ε-aminohexanoate

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Technology Process of benzyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-ε-aminohexanoate

There total 6 articles about benzyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-ε-aminohexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.5%

: 5514-99-8
6-amino-hexanoic acid benzyl ester toluene-4-sulfonic acid

: 87919-03-7
6',6''-di-tert-butyl-18β-glycyrrhizin

: 87919-07-1
benzyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-ε-aminohexanoate

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; 5 degC, 1 h; 12 h, r.t.;

Reference yield:

: 50867-21-5
N,N'-dicylohexylcarbamimidic acid tert-butyl ester

: 87919-07-1
benzyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-ε-aminohexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 11.5 percent / CuCl / CHCl₃; dimethylformamide / 72 h / Ambient temperature

2: 85.5 percent / diethyl phosphorylcyanide, triethylamine / dimethylformamide / 5 degC, 1 h; 12 h, r.t.

With diethyl cyanophosphonate; triethylamine; copper(l) chloride; In chloroform; N,N-dimethyl-formamide;

Reference yield:

: 83896-44-0,103000-77-7,119479-05-9,142394-43-2,1405-86-3
glycyrrizhin

: 87919-07-1
benzyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-ε-aminohexanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 22.6 percent / CHCl₃; dimethylformamide / 72 h / Ambient temperature

2: 76.5 percent / 5percent potassium hydroxide / methanol / 4 h / Ambient temperature

3: 38 percent / CuCl, dicyclohexylcarbodiimide / CHCl₃; dimethylformamide / 72 h / Ambient temperature

4: 90 percent / hydrogen / 5percent Pd-carbon / ethyl acetate / 760 Torr

5: 85.5 percent / diethyl phosphorylcyanide, triethylamine / dimethylformamide / 5 degC, 1 h; 12 h, r.t.

With potassium hydroxide; diethyl cyanophosphonate; hydrogen; triethylamine; dicyclohexyl-carbodiimide; copper(l) chloride; palladium on activated charcoal; In methanol; chloroform; ethyl acetate; N,N-dimethyl-formamide;