2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-6-(trimethylsilyl)phenyl N,N-diethylcarbamate

Base Information

Chemical Name:2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-6-(trimethylsilyl)phenyl N,N-diethylcarbamate
CAS No.:741695-78-3
Molecular Formula:C₂₀H₃₄BNO₄Si
Molecular Weight:391.391
Hs Code.:

Synonyms:2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-6-(trimethylsilyl)phenyl N,N-diethylcarbamate

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Chemical Property of 2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-6-(trimethylsilyl)phenyl N,N-diethylcarbamate

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Technology Process of 2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-6-(trimethylsilyl)phenyl N,N-diethylcarbamate

There total 1 articles about 2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-6-(trimethylsilyl)phenyl N,N-diethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 2,6-bis(trimethylsilyl)phenyl N,N-diethylcarbamate

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 741695-78-3
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-6-(trimethylsilyl)phenyl N,N-diethylcarbamate

Guidance literature:: 2,6-bis(trimethylsilyl)phenyl N,N-diethylcarbamate; With boron tribromide; In dichloromethane; at 20 ℃; for 2h;

2,3-dimethyl-2,3-butane diol; In ethyl acetate;
DOI:10.1021/ol0506563

Reference yield: 56.0%

: 7436-90-0
2,2-dibromostyrene

: 741695-78-3
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-6-(trimethylsilyl)phenyl N,N-diethylcarbamate

: 741695-79-4
Diethyl-carbamic acid 2-((Z)-1-bromo-2-phenyl-vinyl)-6-trimethylsilanyl-phenyl ester

Guidance literature:: With sodium carbonate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In 1,2-dimethoxyethane; water; Heating;
DOI:10.1021/ol049740t

Reference yield:

: 741695-78-3
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-6-(trimethylsilyl)phenyl N,N-diethylcarbamate

: 4645-16-3
3-[1-phenyl-methylidine]-3H-benzofuran-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / TFP; Na₂CO₃ / Pd₂(dba)3 / H₂O; 1,2-dimethoxy-ethane / Heating

2: 96 percent / n-BuLi / tetrahydrofuran / -78 - -30 °C

3: 58 percent / TFA / 24 h / Heating

With n-butyllithium; sodium carbonate; trifluoroacetic acid; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; 1,2-dimethoxyethane; water; 1: Suzuki-Miyaura coupling;
DOI:10.1021/ol049740t