2-[5-chloro-4'-(pyridin-2-yl)biphenyl-3-yl]-4,6-diphenyl-1,3,5-triazine

Base Information

Chemical Name:2-[5-chloro-4'-(pyridin-2-yl)biphenyl-3-yl]-4,6-diphenyl-1,3,5-triazine
CAS No.:1073062-46-0
Molecular Formula:C₃₂H₂₁ClN₄
Molecular Weight:496.999
Hs Code.:

Synonyms:2-[5-chloro-4'-(pyridin-2-yl)biphenyl-3-yl]-4,6-diphenyl-1,3,5-triazine

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Chemical Property of 2-[5-chloro-4'-(pyridin-2-yl)biphenyl-3-yl]-4,6-diphenyl-1,3,5-triazine

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Technology Process of 2-[5-chloro-4'-(pyridin-2-yl)biphenyl-3-yl]-4,6-diphenyl-1,3,5-triazine

There total 3 articles about 2-[5-chloro-4'-(pyridin-2-yl)biphenyl-3-yl]-4,6-diphenyl-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1073062-42-6
2-(3-bromo-5-chlorophenyl )-4,6-diphenyl-1,3,5-triazine

: 170230-27-0
(4-(pyridin-2-yl)phenyl)boronic acid

: 1073062-46-0
2-[5-chloro-4'-(pyridin-2-yl)biphenyl-3-yl]-4,6-diphenyl-1,3,5-triazine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydroxide; In tetrahydrofuran; water; for 16h; Inert atmosphere; Reflux;

Reference yield:

: 1073062-42-6
2-(3-bromo-5-chlorophenyl )-4,6-diphenyl-1,3,5-triazine

: 1073062-44-8
C₁₁H₈ClNZn

: 1073062-46-0
2-[5-chloro-4'-(pyridin-2-yl)biphenyl-3-yl]-4,6-diphenyl-1,3,5-triazine

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; for 18h; Reflux;

Reference yield:

: 188813-05-0
3-bromo-5-chloro-benzaldehyde

: 1073062-46-0
2-[5-chloro-4'-(pyridin-2-yl)biphenyl-3-yl]-4,6-diphenyl-1,3,5-triazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium phosphate / dimethyl sulfoxide / 1 h / 90 °C

1.2: 0.17 h / 20 °C

2.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 3 h / Reflux

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; dimethyl sulfoxide;