2-(3-broMo-5-chlorophenyl)-4,6-diphenyl-1,3,5-triazine

Base Information

• Chemical Name: 2-(3-broMo-5-chlorophenyl)-4,6-diphenyl-1,3,5-triazine
• CAS No.: 1073062-42-6
• Molecular Formula: C21H13BrClN3
• Molecular Weight: 422.711
• Mol file: 1073062-42-6.mol

Synonyms:2-(3-broMo-5-chlorophenyl)-4,6-diphenyl-1,3,5-triazine

Chemical Property of 2-(3-broMo-5-chlorophenyl)-4,6-diphenyl-1,3,5-triazine

Chemical Property:

• Boiling Point: 608.5±65.0 °C(Predicted)
• PKA: 0.21±0.10(Predicted)
• PSA: 38.67000
• Density: 1.442±0.06 g/cm3(Predicted)
• LogP: 6.28850
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

2-(3-Bromo-5-chlorophenyl)-4,6-diphenyl-1,3,5-triazine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(3-broMo-5-chlorophenyl)-4,6-diphenyl-1,3,5-triazine

There total 10 articles about 2-(3-broMo-5-chlorophenyl)-4,6-diphenyl-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

N-(3-bromo-5-chlorobenzoyl)benzamidine + benzamidine monohydrochloride (1670-14-0) → 2-(3-bromo-5-chlorophenyl )-4,6-diphenyl-1,3,5-triazine (1073062-42-6)

Guidance literature:

With sodium carbonate; 2,2,4,4,6,6-hexamethylcyclotrisilazane; In 5,5-dimethyl-1,3-cyclohexadiene; at 150 ℃; for 6h; Solvent; Reagent/catalyst; Inert atmosphere;

Reference yield: 87.0%

3-bromo-5-chloro-benzaldehyde (188813-05-0) + benzamidine monohydrochloride (1670-14-0) → 2-(3-bromo-5-chlorophenyl )-4,6-diphenyl-1,3,5-triazine (1073062-42-6)

Guidance literature:

3-bromo-5-chloro-benzaldehyde; benzamidine monohydrochloride; With potassium phosphate; In dimethyl sulfoxide; at 90 ℃; for 1h;

With magnesium sulfate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dimethyl sulfoxide; at 20 ℃; for 0.166667h;

Reference yield: 84.0%

1-bromo-3-chloro-5-iodobenzene (13101-40-1) + 2,4-diphenyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-1,3,5-triazine → 2-(3-bromo-5-chlorophenyl )-4,6-diphenyl-1,3,5-triazine (1073062-42-6)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; In ethanol; water; toluene; for 5h; Inert atmosphere; Reflux;

upstream raw materials:

3-bromo-5-chloro-benzaldehyde

benzamidine monohydrochloride

phenylmagnesium bromide

1,3-dibromo-5-chlorobenzene

Downstream raw materials:

2-[5-chloro-4'-(pyridin-2-yl)biphenyl-3-yl]-4,6-diphenyl-1,3,5-triazine

2-[3-chloro-5-(phenanthrene-9-yl)phenyl]-4,6-diphenyl-1,3,5-triazine

2-[3-{(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl}-5-(9-phenanthryl)phenyl]-4,6-diphenyl-1,3,5-triazine