2,4-dichloro-6-[3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-pyrazol-1-yl]-[1,3,5]triazine

Base Information

• Chemical Name: 2,4-dichloro-6-[3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-pyrazol-1-yl]-[1,3,5]triazine
• CAS No.: 870009-68-0
• Molecular Formula: C₁₅H₁₃Cl₂N₅O₂S
• Molecular Weight: 398.273

Synonyms:2,4-dichloro-6-[3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-pyrazol-1-yl]-[1,3,5]triazine

Chemical Property of 2,4-dichloro-6-[3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-pyrazol-1-yl]-[1,3,5]triazine

Chemical Property:

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Technology Process of 2,4-dichloro-6-[3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-pyrazol-1-yl]-[1,3,5]triazine

There total 2 articles about 2,4-dichloro-6-[3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-pyrazol-1-yl]-[1,3,5]triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3,4-dimethoxyphenyl)-3,3-bis-methylsulfanyl-propenone (870009-66-8) → 2,4-dichloro-6-[3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-pyrazol-1-yl]-[1,3,5]triazine (870009-68-0)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / Heating

2: K₂CO₃ / tetrahydrofuran / Heating

With potassium carbonate; hydrazine hydrate; In tetrahydrofuran; methanol;

DOI:10.1016/j.bmcl.2005.08.023

Reference yield:

3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-1H-pyrazole (870009-67-9) + 1,3,5-trichloro-2,4,6-triazine (108-77-0) → 2,4-dichloro-6-[3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-pyrazol-1-yl]-[1,3,5]triazine (870009-68-0)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; Heating;

DOI:10.1016/j.bmcl.2005.08.023

Reference yield: 65.0%

2,4-dichloro-6-[3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-pyrazol-1-yl]-[1,3,5]triazine (870009-68-0) + o-toluidine (95-53-4) → 6-[3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-pyrazol-1-yl]-N,N'-di-o-tolyl-[1,3,5]triazine-2,4-diamine

Guidance literature:

With potassium carbonate; In tetrahydrofuran; Heating;

DOI:10.1016/j.bmcl.2005.08.023

upstream raw materials:

3-(3,4-dimethoxy-phenyl)-5-methylsulfanyl-1H-pyrazole

1,3,5-trichloro-2,4,6-triazine

1-(3,4-dimethoxyphenyl)-3,3-bis-methylsulfanyl-propenone

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