[(3-methoxyphenyl)methyl]-(4-trimethylsilyl-3-butynyl)propanedioic acid diethyl ester

Base Information

Chemical Name:[(3-methoxyphenyl)methyl]-(4-trimethylsilyl-3-butynyl)propanedioic acid diethyl ester
CAS No.:288632-75-7
Molecular Formula:C₂₂H₃₂O₅Si
Molecular Weight:404.579
Hs Code.:

Synonyms:[(3-methoxyphenyl)methyl]-(4-trimethylsilyl-3-butynyl)propanedioic acid diethyl ester

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Chemical Property of [(3-methoxyphenyl)methyl]-(4-trimethylsilyl-3-butynyl)propanedioic acid diethyl ester

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Technology Process of [(3-methoxyphenyl)methyl]-(4-trimethylsilyl-3-butynyl)propanedioic acid diethyl ester

There total 3 articles about [(3-methoxyphenyl)methyl]-(4-trimethylsilyl-3-butynyl)propanedioic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 288632-74-6
(4-trimethylsilyl-3-butynyl)propanedioic acid diethyl ester

: 824-98-6
m-methoxybenzyl chloride

: 288632-75-7
[(3-methoxyphenyl)methyl]-(4-trimethylsilyl-3-butynyl)propanedioic acid diethyl ester

Guidance literature:: (4-trimethylsilyl-3-butynyl)propanedioic acid diethyl ester; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;

m-methoxybenzyl chloride; In tetrahydrofuran; at 40 ℃; for 12h; Further stages.;
DOI:10.1021/jo000255v

Reference yield:

: 41423-29-4
4-iodo-1-butynyltrimethylsilane

: 288632-75-7
[(3-methoxyphenyl)methyl]-(4-trimethylsilyl-3-butynyl)propanedioic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 0 - 20 °C

1.2: 49 percent / tetrahydrofuran / 24 h / 20 °C

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: tetrahydrofuran / 12 h / 40 °C

With sodium hydride; In tetrahydrofuran; 1.1: Substitution / 1.2: Alkylation / 2.1: Substitution / 2.2: Alkylation;
DOI:10.1021/jo000255v

Reference yield:

: 105-53-3
diethyl malonate

: 288632-75-7
[(3-methoxyphenyl)methyl]-(4-trimethylsilyl-3-butynyl)propanedioic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 0 - 20 °C

1.2: 49 percent / tetrahydrofuran / 24 h / 20 °C

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: tetrahydrofuran / 12 h / 40 °C

With sodium hydride; In tetrahydrofuran; 1.1: Substitution / 1.2: Alkylation / 2.1: Substitution / 2.2: Alkylation;
DOI:10.1021/jo000255v