3-carbamoyl-1-carbamoylmethyl>-1,4-dihydropyridine

Base Information

Chemical Name:3-carbamoyl-1-carbamoylmethyl>-1,4-dihydropyridine
CAS No.:97559-27-8
Molecular Formula:C₁₆H₁₉N₃O₂
Molecular Weight:285.346
Hs Code.:

3-carbamoyl-1-<N-<β-(phenyl)ethyl>carbamoylmethyl>-1,4-dihydropyridine

Synonyms:3-carbamoyl-1-carbamoylmethyl>-1,4-dihydropyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-carbamoyl-1-carbamoylmethyl>-1,4-dihydropyridine

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Technology Process of 3-carbamoyl-1-carbamoylmethyl>-1,4-dihydropyridine

There total 5 articles about 3-carbamoyl-1-carbamoylmethyl>-1,4-dihydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 3-carbamoyl-1-carbamoylmethyl>pyridinium bromide

: 97559-27-8
3-carbamoyl-1-carbamoylmethyl>-1,4-dihydropyridine

Guidance literature:: With sodium dithionite; sodium hydrogencarbonate; In methanol; water; at 0 ℃; for 1h;
DOI:10.1002/jps.2600740304

Reference yield:

: 64297-92-3
N-(β-phenethyl)-2-bromoacetamide

: 97559-27-8
3-carbamoyl-1-carbamoylmethyl>-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / acetonitrile / 96 h / Heating

2: 84 percent / NaHCO₃, sodium dithionite / H₂O; methanol / 1 h / 0 °C

With sodium dithionite; sodium hydrogencarbonate; In methanol; water; acetonitrile;
DOI:10.1002/jps.2600740304

Reference yield:

: 98-92-0,1255150-40-3
nicotinamide

: 97559-27-8
3-carbamoyl-1-carbamoylmethyl>-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / acetonitrile / 96 h / Heating

2: 84 percent / NaHCO₃, sodium dithionite / H₂O; methanol / 1 h / 0 °C

With sodium dithionite; sodium hydrogencarbonate; In methanol; water; acetonitrile;
DOI:10.1002/jps.2600740304