diphenyl methyl sulfinylacetamide

Base Information

• Chemical Name: diphenyl methyl sulfinylacetamide
• CAS No.: 79388-17-3
• Molecular Formula: C₁₅H₁₅NO₂S
• Molecular Weight: 273.356
• Mol file: 79388-17-3.mol

Synonyms:diphenyl methyl sulfinylacetamide

Chemical Property of diphenyl methyl sulfinylacetamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of diphenyl methyl sulfinylacetamide

There total 2 articles about diphenyl methyl sulfinylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-phenyl-α-(methylthio)acetanilide (79388-14-0) → diphenyl methyl sulfinylacetamide (79388-17-3)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1.) 0 deg C, 2.) room temp., 1 h;

DOI:10.1055/s-1981-29515

Reference yield:

diphenylamine (122-39-4) → diphenyl methyl sulfinylacetamide (79388-17-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / triethylamine / CH₂Cl₂ / 3 h / Heating

2: 94 percent / 3-chlorobenzoperoxoic acid / CH₂Cl₂ / 1.) 0 deg C, 2.) room temp., 1 h

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1055/s-1981-29515

Reference yield: 86.0%

diphenyl methyl sulfinylacetamide (79388-17-3) → 3-(methylthio)-1-phenylindolin-2-one (79388-20-8)

Guidance literature:

With toluene-4-sulfonic acid; In tetrachloromethane; for 0.333333h; Heating;

DOI:10.1055/s-1981-29515

upstream raw materials:

N-phenyl-α-(methylthio)acetanilide

diphenylamine

Downstream raw materials:

3-(methylthio)-1-phenylindolin-2-one

1-phenyl-1,3-dihydro-indol-2-one