methyl 2-(4-carbamimidoylphenoxy)-2-(3-ethoxy-4-isopropoxyphenyl)acetate acetate

Base Information

Chemical Name:methyl 2-(4-carbamimidoylphenoxy)-2-(3-ethoxy-4-isopropoxyphenyl)acetate acetate
CAS No.:948992-47-0
Molecular Formula:C₂H₄O₂*C₂₁H₂₆N₂O₅
Molecular Weight:446.5
Hs Code.:

Synonyms:methyl 2-(4-carbamimidoylphenoxy)-2-(3-ethoxy-4-isopropoxyphenyl)acetate acetate

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Chemical Property of methyl 2-(4-carbamimidoylphenoxy)-2-(3-ethoxy-4-isopropoxyphenyl)acetate acetate

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Technology Process of methyl 2-(4-carbamimidoylphenoxy)-2-(3-ethoxy-4-isopropoxyphenyl)acetate acetate

There total 4 articles about methyl 2-(4-carbamimidoylphenoxy)-2-(3-ethoxy-4-isopropoxyphenyl)acetate acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 948992-45-8
methyl 2-(4-(N-hydroxycarbamimidoyl)phenoxy)-2-(3-ethoxy-4-isopropoxyphenyl)acetate

: 64-19-7,77671-22-8
acetic acid

: 948992-47-0
methyl 2-(4-carbamimidoylphenoxy)-2-(3-ethoxy-4-isopropoxyphenyl)acetate acetate

Guidance literature:: With hydrogen; acetic anhydride; palladium 10% on activated carbon; at 20 ℃; for 3h;

Reference yield:

: 948992-44-7
methyl 2-(4-cyanophenoxy)-2-(3-ethoxy-4-isopropoxyphenyl)acetate

: 948992-47-0
methyl 2-(4-carbamimidoylphenoxy)-2-(3-ethoxy-4-isopropoxyphenyl)acetate acetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; triethylamine / dimethyl sulfoxide / 18.17 h / 20 - 60 °C

2: hydrogen; acetic anhydride / palladium 10% on activated carbon / 3 h / 20 °C

With hydroxylamine hydrochloride; hydrogen; acetic anhydride; triethylamine; palladium 10% on activated carbon; In dimethyl sulfoxide;

Reference yield:

: 745019-93-6
methyl 2-(3-ethoxy-4-isopropoxyphenyl)-2-hydroxyacetate

: 948992-47-0
methyl 2-(4-carbamimidoylphenoxy)-2-(3-ethoxy-4-isopropoxyphenyl)acetate acetate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 18 h / 20 °C

2: hydroxylamine hydrochloride; triethylamine / dimethyl sulfoxide / 18.17 h / 20 - 60 °C

3: hydrogen; acetic anhydride / palladium 10% on activated carbon / 3 h / 20 °C

With hydroxylamine hydrochloride; hydrogen; acetic anhydride; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium 10% on activated carbon; In tetrahydrofuran; dimethyl sulfoxide; 1: Mitsunobu reaction;