(3-Methylideneazetidin-1-yl)(phenyl)methanone

Base Information

Chemical Name:(3-Methylideneazetidin-1-yl)(phenyl)methanone
CAS No.:222527-63-1
Molecular Formula:C11H11 N O
Molecular Weight:0
Hs Code.:
DSSTox Substance ID:DTXSID30445309
Nikkaji Number:J1.092.469C
Wikidata:Q82263676
Mol file:222527-63-1.mol

Synonyms:222527-63-1;(3-Methylideneazetidin-1-yl)(phenyl)methanone;1-Benzoyl-3-methyleneazetidine;DTXSID30445309

Suppliers and Price of (3-Methylideneazetidin-1-yl)(phenyl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of (3-Methylideneazetidin-1-yl)(phenyl)methanone

Chemical Property:

PSA：20.31000
LogP:1.63650
XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:173.084063974
Heavy Atom Count:13
Complexity:220

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C1CN(C1)C(=O)C2=CC=CC=C2

Technology Process of (3-Methylideneazetidin-1-yl)(phenyl)methanone

There total 2 articles about (3-Methylideneazetidin-1-yl)(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 222527-61-9
N-benzoyl-3-(bromomethyl)-3-chloroazetidine

: 222527-63-1
N-benzoyl-3-methyleneazetidine

Guidance literature:: With zinc; In tetrahydrofuran; at 65 ℃; for 12h;
DOI:10.1080/00397919908086047

Reference yield:

: 98-88-4
benzoyl chloride

: 222527-63-1
N-benzoyl-3-methyleneazetidine

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / NaOH / diethyl ether / 12 h / 0 - 20 °C

2: 88 percent / activated Zn / tetrahydrofuran / 12 h / 65 °C

With sodium hydroxide; zinc; In tetrahydrofuran; diethyl ether;
DOI:10.1080/00397919908086047