1-ethylthio-9,10-dioxo-9,10-dihydroanthracene-2-carboxanilide

Base Information

• Chemical Name: 1-ethylthio-9,10-dioxo-9,10-dihydroanthracene-2-carboxanilide
• CAS No.: 430433-68-4
• Molecular Formula: C₂₃H₁₇NO₃S
• Molecular Weight: 387.459
• Mol file: 430433-68-4.mol

Synonyms:1-ethylthio-9,10-dioxo-9,10-dihydroanthracene-2-carboxanilide

Chemical Property of 1-ethylthio-9,10-dioxo-9,10-dihydroanthracene-2-carboxanilide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-ethylthio-9,10-dioxo-9,10-dihydroanthracene-2-carboxanilide

There total 3 articles about 1-ethylthio-9,10-dioxo-9,10-dihydroanthracene-2-carboxanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1-nitro-9,10-dioxo-9,10-dihydroanthracene-2-carboxanilide (80685-64-9) + sodium thioethylate (811-51-8) → 1-ethylthio-9,10-dioxo-9,10-dihydroanthracene-2-carboxanilide (430433-68-4)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1023/A:1013003122428

Reference yield:

1-nitroanthraquinone-2-carboxylic acid (128-67-6) → 1-ethylthio-9,10-dioxo-9,10-dihydroanthracene-2-carboxanilide (430433-68-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / thionyl chloride; N,N-dimethylformamide / benzene / 3 h / 80 °C

2: 84 percent / H₂O; benzene / 2 h / 15 °C

3: 86 percent / dimethylformamide / 20 °C

With thionyl chloride; N,N-dimethyl-formamide; In water; N,N-dimethyl-formamide; benzene;

DOI:10.1023/A:1013003122428

Reference yield:

1-nitro-9,10-dioxo-9,10-dihydroanthracene-2-carbonyl chloride (602-10-8) → 1-ethylthio-9,10-dioxo-9,10-dihydroanthracene-2-carboxanilide (430433-68-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 84 percent / H₂O; benzene / 2 h / 15 °C

2: 86 percent / dimethylformamide / 20 °C

In water; N,N-dimethyl-formamide; benzene;

DOI:10.1023/A:1013003122428

upstream raw materials:

1-nitro-9,10-dioxo-9,10-dihydroanthracene-2-carboxanilide

sodium thioethylate

1-nitro-9,10-dioxo-9,10-dihydroanthracene-2-carbonyl chloride

1-nitroanthraquinone-2-carboxylic acid

Downstream raw materials:

2-phenyl-2,3,6,11-tetrahydroanthra[2,1-d]isothiazole-3,6,11-trione