Technology Process of C23H24F2N6
There total 10 articles about C23H24F2N6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutylammomium bromide; potassium hydroxide;
In
2-methyltetrahydrofuran; water;
at 50 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / water; 1,4-dioxane / 16 h / 110 °C / Inert atmosphere
2.1: sodium hydroxide; hydrogen / ethanol; water; tetrahydrofuran / 40 h / 50 °C / 750.08 Torr
3.1: hydrogenchloride / water; 1,4-dioxane / 3 h / 80 °C
3.2: pH 9
4.1: trichlorophosphate / chloroform / 3 h / Reflux
5.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C
5.2: 0 - 20 °C
6.1: potassium hydroxide; tetrabutylammomium bromide / water; 2-methyltetrahydrofuran / 50 °C
With
hydrogenchloride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; tetrabutylammomium bromide; hydrogen; sodium carbonate; potassium hydroxide; sodium hydroxide; lithium hexamethyldisilazane; trichlorophosphate;
In
tetrahydrofuran; 2-methyltetrahydrofuran; 1,4-dioxane; ethanol; chloroform; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydroxide; hydrogen / ethanol; water; tetrahydrofuran / 40 h / 50 °C / 750.08 Torr
2.1: hydrogenchloride / water; 1,4-dioxane / 3 h / 80 °C
2.2: pH 9
3.1: trichlorophosphate / chloroform / 3 h / Reflux
4.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C
4.2: 0 - 20 °C
5.1: potassium hydroxide; tetrabutylammomium bromide / water; 2-methyltetrahydrofuran / 50 °C
With
hydrogenchloride; tetrabutylammomium bromide; hydrogen; potassium hydroxide; sodium hydroxide; lithium hexamethyldisilazane; trichlorophosphate;
In
tetrahydrofuran; 2-methyltetrahydrofuran; 1,4-dioxane; ethanol; chloroform; water;